(2S,3S)-2-benzyl-3-hydroxy-2-methylcyclohexanone

Base Information

Chemical Name:(2S,3S)-2-benzyl-3-hydroxy-2-methylcyclohexanone
CAS No.:1187848-75-4
Molecular Formula:C₁₄H₁₈O₂
Molecular Weight:218.296
Hs Code.:

Synonyms:(2S,3S)-2-benzyl-3-hydroxy-2-methylcyclohexanone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S)-2-benzyl-3-hydroxy-2-methylcyclohexanone

Chemical Property:

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Technology Process of (2S,3S)-2-benzyl-3-hydroxy-2-methylcyclohexanone

There total 8 articles about (2S,3S)-2-benzyl-3-hydroxy-2-methylcyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 127311-61-9
2-benzyl-2-methyl-cyclohexane-1,3-dione

: 1187848-75-4
(2S,3S)-2-benzyl-3-hydroxy-2-methylcyclohexanone

Guidance literature:: With C₄₂H₅₁F₅NO₃P; N-ethyl-N,N-diisopropylamine; benzo[1,3,2]dioxaborole; In dichloromethane; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jacs.1c00277

Reference yield:

: 127311-61-9
2-benzyl-2-methyl-cyclohexane-1,3-dione

: 1187848-75-4
(2S,3S)-2-benzyl-3-hydroxy-2-methylcyclohexanone

: 2-benzyl-2-methylcyclohexane-1,3-diol

Guidance literature:: With D-glucose; Bacillus megaterium glucose dehydrogenase; recombinant Ogataea glucozyma ketoreductase KRED₁-Pglu; nicotinamide adenine dinucleotide phosphate; In dimethyl sulfoxide; for 24h; pH=8.0; stereoselective reaction; Enzymatic reaction;
DOI:10.1007/s10562-019-03015-y

Reference yield:

: 2-benzyl-3-hydroxy-2-methylcyclohexanone

: 912653-79-3
(2R,3R)-2-benzyl-3-hydroxy-2-methylcyclohexanone

: C₁₄H₁₈O₂

: 1187848-75-4
(2S,3S)-2-benzyl-3-hydroxy-2-methylcyclohexanone

Guidance literature:: With bis(1,5-cyclooctadiene)diiridium(I) dichloride; f-ampha; hydrogen; sodium t-butanolate; In dichloromethane; at 20 ℃; for 14h; under 30402 Torr; Overall yield = 83 %; stereoselective reaction;
DOI:10.1039/c9sc01769k