1-<2'-deoxy-3'-O-mesyl-5'-O-(4-monomethoxytrityl)-α-D-ribofuranosyl>-6,7-diphenylpteridine-2,4(1H,3H)-dione

Base Information

• Chemical Name: 1-<2'-deoxy-3'-O-mesyl-5'-O-(4-monomethoxytrityl)-α-D-ribofuranosyl>-6,7-diphenylpteridine-2,4(1H,3H)-dione
• CAS No.: 143570-43-8
• Molecular Formula: C₄₄H₃₈N₄O₈S
• Molecular Weight: 782.874

Synonyms:1-<2'-deoxy-3'-O-mesyl-5'-O-(4-monomethoxytrityl)-α-D-ribofuranosyl>-6,7-diphenylpteridine-2,4(1H,3H)-dione

Chemical Property of 1-<2'-deoxy-3'-O-mesyl-5'-O-(4-monomethoxytrityl)-α-D-ribofuranosyl>-6,7-diphenylpteridine-2,4(1H,3H)-dione

Chemical Property:

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Technology Process of 1-<2'-deoxy-3'-O-mesyl-5'-O-(4-monomethoxytrityl)-α-D-ribofuranosyl>-6,7-diphenylpteridine-2,4(1H,3H)-dione

There total 1 articles about 1-<2'-deoxy-3'-O-mesyl-5'-O-(4-monomethoxytrityl)-α-D-ribofuranosyl>-6,7-diphenylpteridine-2,4(1H,3H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1-<2'-deoxy-5'-O-(4-monomethoxytrityl)-α-D-ribofuranosyl>-6,7-diphenylpteridine-2,4(1H,3H)-dione (71470-96-7) + methanesulfonyl chloride (124-63-0) → 1-<2'-deoxy-3'-O-mesyl-5'-O-(4-monomethoxytrityl)-α-D-ribofuranosyl>-6,7-diphenylpteridine-2,4(1H,3H)-dione (143570-43-8)

Guidance literature:

With pyridine; for 19h;

DOI:10.1002/hlca.19920750427

Reference yield: 82.0%

1-<2'-deoxy-3'-O-mesyl-5'-O-(4-monomethoxytrityl)-α-D-ribofuranosyl>-6,7-diphenylpteridine-2,4(1H,3H)-dione (143570-43-8) → 1-<2',3'-didehydro-2',3'-dideoxy-5'-O-(4-monomethoxytrityl)-α-D-glycero-pentofuranosyl>-6,7-diphenylpteridine-2,4(1H,3H)-dione (143570-45-0)

Guidance literature:

With potassium tert-butylate; In N,N-dimethyl-formamide; tert-butyl alcohol; at 90 ℃; for 1h;

DOI:10.1002/hlca.19920750427

Reference yield: 82.0%

1-<2'-deoxy-3'-O-mesyl-5'-O-(4-monomethoxytrityl)-α-D-ribofuranosyl>-6,7-diphenylpteridine-2,4(1H,3H)-dione (143570-43-8) → 1-(2'-deoxy-3'-O-mesyl-α-D-ribofuranosyl)-6,7-diphenylpteridine-2,4(1H,3H)-dione (143570-44-9)

Guidance literature:

With toluene-4-sulfonic acid; In methanol; dichloromethane; for 2h;

DOI:10.1002/hlca.19920750427

upstream raw materials:

1-<2'-deoxy-5'-O-(4-monomethoxytrityl)-α-D-ribofuranosyl>-6,7-diphenylpteridine-2,4(1H,3H)-dione

methanesulfonyl chloride

Downstream raw materials:

1-(2'-deoxy-3'-O-mesyl-α-D-ribofuranosyl)-6,7-diphenylpteridine-2,4(1H,3H)-dione

1-<2',3'-didehydro-2',3'-dideoxy-5'-O-(4-monomethoxytrityl)-α-D-glycero-pentofuranosyl>-6,7-diphenylpteridine-2,4(1H,3H)-dione

1-(3',5'-anhydro-2'-deoxy-α-D-xylofuranosyl)-6,7-diphenylpteridine-2,4(1H,3H)-dione

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