MIDA alkenyl-2-boronate

Base Information

Chemical Name:MIDA alkenyl-2-boronate
CAS No.:1311484-52-2
Molecular Formula:C₁₃H₁₄BNO₄
Molecular Weight:259.069
Hs Code.:

Synonyms:MIDA alkenyl-2-boronate

Suppliers and Price of MIDA alkenyl-2-boronate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of MIDA alkenyl-2-boronate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of MIDA alkenyl-2-boronate

There total 6 articles about MIDA alkenyl-2-boronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1449377-16-5
C₇H₉BBrNO₄

: 98-80-6
phenylboronic acid

: 1311484-52-2
MIDA alkenyl-2-boronate

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,6-bis(diphenylphosphino)hexane; silver carbonate; In tetrahydrofuran; at 40 ℃; for 24h; Sealed tube; Inert atmosphere;
DOI:10.1016/j.tet.2013.05.050

Reference yield:

: 1449377-16-5
C₇H₉BBrNO₄

: 98-80-6
phenylboronic acid

: (E)-6-methyl-2-styryl-1,3,6,2-dioxazaborocane-4,8-dione

: 1311484-52-2
MIDA alkenyl-2-boronate

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 1,5-bis-(diphenylphosphino)pentane; silver carbonate; In tetrahydrofuran; at 40 ℃; for 24h; Reagent/catalyst; Catalytic behavior; Sealed tube; Inert atmosphere;
DOI:10.1016/j.tet.2013.05.050

Reference yield:

: 536-74-3
phenylacetylene

: (E)-6-methyl-2-styryl-1,3,6,2-dioxazaborocane-4,8-dione

: 1311484-52-2
MIDA alkenyl-2-boronate

Guidance literature:: Multi-step reaction with 3 steps

1: 24 h / 20 °C / Inert atmosphere

2: water / Inert atmosphere

3: toluene; dimethyl sulfoxide / 16 h / 20 °C / Inert atmosphere; Dean-Stark

With water; In dimethyl sulfoxide; toluene;
DOI:10.1002/ejic.202000229