tert-butyl 2-(3-(2-(4-(3,5-dichlorobenzoyl)piperazin-1-yl)ethylamino)propyl)-1H-benzo[d]imidazole-1-carboxylate

Base Information

Chemical Name:tert-butyl 2-(3-(2-(4-(3,5-dichlorobenzoyl)piperazin-1-yl)ethylamino)propyl)-1H-benzo[d]imidazole-1-carboxylate
CAS No.:1355016-67-9
Molecular Formula:C₂₈H₃₅Cl₂N₅O₃
Molecular Weight:560.524
Hs Code.:

Synonyms:tert-butyl 2-(3-(2-(4-(3,5-dichlorobenzoyl)piperazin-1-yl)ethylamino)propyl)-1H-benzo[d]imidazole-1-carboxylate

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Chemical Property of tert-butyl 2-(3-(2-(4-(3,5-dichlorobenzoyl)piperazin-1-yl)ethylamino)propyl)-1H-benzo[d]imidazole-1-carboxylate

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Technology Process of tert-butyl 2-(3-(2-(4-(3,5-dichlorobenzoyl)piperazin-1-yl)ethylamino)propyl)-1H-benzo[d]imidazole-1-carboxylate

There total 6 articles about tert-butyl 2-(3-(2-(4-(3,5-dichlorobenzoyl)piperazin-1-yl)ethylamino)propyl)-1H-benzo[d]imidazole-1-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₃₃Cl₂N₅O₃

: 1355016-67-9
tert-butyl 2-(3-(2-(4-(3,5-dichlorobenzoyl)piperazin-1-yl)ethylamino)propyl)-1H-benzo[d]imidazole-1-carboxylate

Guidance literature:: With sodium tris(acetoxy)borohydride; In methanol; for 6h;
DOI:10.1016/j.bmc.2011.11.005

Reference yield:

: 1355016-60-2
2-(2-(4-(3,5-dichlorobenzoyl)piperazin-1-yl)ethyl)isoindoline-1,3-dione

: 1355016-67-9
tert-butyl 2-(3-(2-(4-(3,5-dichlorobenzoyl)piperazin-1-yl)ethylamino)propyl)-1H-benzo[d]imidazole-1-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine hydrate / ethanol / 2 h / 60 °C

2: methanol / 2 h

3: sodium tris(acetoxy)borohydride / methanol / 6 h

With sodium tris(acetoxy)borohydride; hydrazine hydrate; In methanol; ethanol;
DOI:10.1016/j.bmc.2011.11.005

Reference yield:

: 1355016-62-4
(4-(2-aminoethyl)piperazin-1-yl)(3,5-dichlorophenyl)methanone

: 1355016-67-9
tert-butyl 2-(3-(2-(4-(3,5-dichlorobenzoyl)piperazin-1-yl)ethylamino)propyl)-1H-benzo[d]imidazole-1-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 2 h

2: sodium tris(acetoxy)borohydride / methanol / 6 h

With sodium tris(acetoxy)borohydride; In methanol;
DOI:10.1016/j.bmc.2011.11.005