C₃₃H₄₅NO₄SSi

Base Information

Chemical Name:C₃₃H₄₅NO₄SSi
CAS No.:127354-70-5
Molecular Formula:C₃₃H₄₅NO₄SSi
Molecular Weight:579.876
Hs Code.:

C<sub>33</sub>H<sub>45</sub>NO<sub>4</sub>SSi

Synonyms:C₃₃H₄₅NO₄SSi

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Chemical Property of C₃₃H₄₅NO₄SSi

Chemical Property:

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Technology Process of C₃₃H₄₅NO₄SSi

There total 3 articles about C₃₃H₄₅NO₄SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 114634-56-9
C₃₂H₄₃NO₄SSi

: 127354-70-5
C₃₃H₄₅NO₄SSi

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / (dimethylamino)pyridine (DMAP), diazabicycloundecene (DBU) / acetonitrile / 4 h / Ambient temperature

2: 1.) lithium hexamethyldisilazide / 1.) THF, from -78 deg C to -40 deg C, 10 min, 2.) -78 deg C to 20 deg C, 10 min

With dmap; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium hexamethyldisilazane; In acetonitrile;
DOI:10.1021/ja00167a037

Reference yield:

: 114634-55-8
C₃₄H₄₅NO₅SSi

: 127354-70-5
C₃₃H₄₅NO₄SSi

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / K₂CO₃ / tetrahydrofuran; methanol / 0.58 h

2: 76 percent / (dimethylamino)pyridine (DMAP), diazabicycloundecene (DBU) / acetonitrile / 4 h / Ambient temperature

3: 1.) lithium hexamethyldisilazide / 1.) THF, from -78 deg C to -40 deg C, 10 min, 2.) -78 deg C to 20 deg C, 10 min

With dmap; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium hexamethyldisilazane; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1021/ja00167a037

Reference yield:

: 114634-57-0
C₃₈H₅₇NO₄SSi₂

: 74-88-4
methyl iodide

: 127354-70-5
C₃₃H₄₅NO₄SSi

Guidance literature:: With lithium hexamethyldisilazane; Yield given. Multistep reaction; 1.) THF, from -78 deg C to -40 deg C, 10 min, 2.) -78 deg C to 20 deg C, 10 min;
DOI:10.1021/ja00167a037