N-(butylcarbamoyl-phenyl-methyl)-N-(2-hydroxy-ethyl)-2-methanesulfonylamino-benzamide

Base Information

Chemical Name:N-(butylcarbamoyl-phenyl-methyl)-N-(2-hydroxy-ethyl)-2-methanesulfonylamino-benzamide
CAS No.:934421-03-1
Molecular Formula:C₂₂H₂₉N₃O₅S
Molecular Weight:447.555
Hs Code.:

<i>N</i>-(butylcarbamoyl-phenyl-methyl)-<i>N</i>-(2-hydroxy-ethyl)-2-methanesulfonylamino-benzamide

Synonyms:N-(butylcarbamoyl-phenyl-methyl)-N-(2-hydroxy-ethyl)-2-methanesulfonylamino-benzamide

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Chemical Property of N-(butylcarbamoyl-phenyl-methyl)-N-(2-hydroxy-ethyl)-2-methanesulfonylamino-benzamide

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Technology Process of N-(butylcarbamoyl-phenyl-methyl)-N-(2-hydroxy-ethyl)-2-methanesulfonylamino-benzamide

There total 2 articles about N-(butylcarbamoyl-phenyl-methyl)-N-(2-hydroxy-ethyl)-2-methanesulfonylamino-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 2769-64-4
n-butyl isonitrile

: 162787-61-3
2-(methylsulfonamido)benzoic acid

: 124948-51-2
(E)-2-(benzylideneamino)ethanol

: 934421-03-1
N-(butylcarbamoyl-phenyl-methyl)-N-(2-hydroxy-ethyl)-2-methanesulfonylamino-benzamide

Guidance literature:: With 3 A molecular sieve; In methanol; at 20 ℃; for 24h;
DOI:10.1021/jo062626z

Reference yield:

: 100-52-7
benzaldehyde

: 934421-03-1
N-(butylcarbamoyl-phenyl-methyl)-N-(2-hydroxy-ethyl)-2-methanesulfonylamino-benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: molecular sieves 4 Angstroem / diethyl ether / 1 h / 20 °C

2: 57 percent / molecular sieves 3 Angstroem / methanol / 24 h / 20 °C

With 3 A molecular sieve; 4 A molecular sieve; In methanol; diethyl ether; 2: Ugi reaction;
DOI:10.1021/jo062626z