Rh(CO)(P(C₆H₅)3)2((FC₆H₄)2N₃H)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2((FC₆H₄)2N₃H)][BF₄]

Base Information

• Chemical Name: Rh(CO)(P(C₆H₅)3)2((FC₆H₄)2N₃H)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2((FC₆H₄)2N₃H)][BF₄]
• CAS No.: 66540-46-3
• Molecular Formula: BF₄*C₄₉H₃₉F₂N₃OP₂Rh
• Molecular Weight: 975.523

Synonyms:Rh(CO)(P(C₆H₅)3)2((FC₆H₄)2N₃H)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2((FC₆H₄)2N₃H)][BF₄]

Chemical Property of Rh(CO)(P(C₆H₅)3)2((FC₆H₄)2N₃H)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2((FC₆H₄)2N₃H)][BF₄]

Chemical Property:

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Technology Process of Rh(CO)(P(C₆H₅)3)2((FC₆H₄)2N₃H)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2((FC₆H₄)2N₃H)][BF₄]

There total 5 articles about Rh(CO)(P(C₆H₅)3)2((FC₆H₄)2N₃H)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2((FC₆H₄)2N₃H)][BF₄] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

tetrafluoroboric acid + Rh(1+)*CO*2P(C6H5)3*FC6H4NNNC6H4F(1-)=Rh(CO)(P(C6H5)3)2(FC6H4NNNC6H4F) → Rh(CO)(P(C6H5)3)2((FC6H4)2N3H)(1+)*BF4(1-)=[Rh(CO)(P(C6H5)3)2((FC6H4)2N3H)][BF4] (66540-46-3)

Guidance literature:

In diethyl ether; water; N2-atmosphere; dropwise addn. of aq. HBF4 (42 %) to suspn. of Rh-complexin Et2O, stirring (5 min, pptn.); collecting, washing (hexane, Et2O), drying in air, recrystn. (Me2CO/Et2O); elem. anal.;

DOI:10.1039/DT9780000050

Reference yield:

Rh(CO)(P(C6H5)3)2(OC(CH3)2)(1+)*BF4(1-)=[Rh(CO)(P(C6H5)3)2(OC(CH3)2)][BF4] (66609-55-0) → Rh(CO)(P(C6H5)3)2((FC6H4)2N3H)(1+)*BF4(1-)=[Rh(CO)(P(C6H5)3)2((FC6H4)2N3H)][BF4] (66540-46-3)

Guidance literature:

Multi-step reaction with 3 steps

1: not given

2: water; ethanol

3: not given

In ethanol; water;

DOI:10.1039/DT9780000050

Reference yield:

carbonyl(diphenyltriazene)bis(triphenylphosphine)rhodium tetrafluoroborate (66540-42-9) → Rh(CO)(P(C6H5)3)2((FC6H4)2N3H)(1+)*BF4(1-)=[Rh(CO)(P(C6H5)3)2((FC6H4)2N3H)][BF4] (66540-46-3)

Guidance literature:

Multi-step reaction with 2 steps

1: water; ethanol

2: not given

In ethanol; water;

DOI:10.1039/DT9780000050

upstream raw materials:

Rh(CO)(P(C₆H₅)3)2(OC(CH₃)2)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2(OC(CH₃)2)][BF₄]

1,3-bis(4-fluorophenyl)-triazene

carbonyl(diphenyltriazene)bis(triphenylphosphine)rhodium tetrafluoroborate

Rh(CO)(P(C₆H₅)3)2((CH₃C₆H₄)2N₃H)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2((CH₃C₆H₄)2N₃H)][BF₄]

Downstream raw materials:

Rh(CO)(P(C₆H₅)3)2(OC(CH₃)2)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2(OC(CH₃)2)][BF₄]

Rh(CO)(P(C₆H₅)3)2((CH₃C₆H₄)2N₃H)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2((CH₃C₆H₄)2N₃H)][BF₄]

Rh(CO)(P(C₆H₅)3)2I₃

chlorocarbonylbis(triphenylphosphine)rhodium(I)

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