1-Triazene, 1,3-bis(4-fluorophenyl)-

Base Information

• Chemical Name: 1-Triazene, 1,3-bis(4-fluorophenyl)-
• CAS No.: 1524-21-6
• Molecular Formula: C12H9F2N3
• Molecular Weight: 233.22
• DSSTox Substance ID: DTXSID90477242
• Nikkaji Number: J839.876C
• Mol file: 1524-21-6.mol

Synonyms:1524-21-6;1-Triazene, 1,3-bis(4-fluorophenyl)-;1,3-Bis(4-fluorophenyl)triazene;DTXSID90477242;1,3-bis(p-fluorophenyl)-triazene

Chemical Property of 1-Triazene, 1,3-bis(4-fluorophenyl)-

Chemical Property:

• XLogP3: 4.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 3
• Exact Mass: 233.07645362
• Heavy Atom Count: 17
• Complexity: 244

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=CC=C1NN=NC2=CC=C(C=C2)F)F

Technology Process of 1-Triazene, 1,3-bis(4-fluorophenyl)-

There total 3 articles about 1-Triazene, 1,3-bis(4-fluorophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-fluoroaniline (371-40-4) → 1,3-bis(4-fluorophenyl)-triazene (1524-21-6)

Guidance literature:

4-fluoroaniline; With hydrogenchloride; sodium nitrite; In water; for 0.0833333h; Cooling;

With sodium acetate; In water; at 5 - 10 ℃; for 0.833333h;

DOI:10.1002/ejoc.201600891

Reference yield:

p-fluoroaniline hydrochloride (2146-07-8) → 1,3-bis(4-fluorophenyl)-triazene (1524-21-6)

Guidance literature:

Multistep reaction; (i) NaNO₂, aq. HCl, (ii) aq. NaOAc;

DOI:10.1016/S0040-4020(01)99185-9

Reference yield:

→ 1,3-bis(4-fluorophenyl)-triazene (1524-21-6)

Guidance literature:

/BRN= 911504/;

DOI:10.1039/jr9530000700

upstream raw materials:

p-fluoroaniline hydrochloride

4-fluoroaniline

Downstream raw materials:

fluorobenzene

1-(4-fluorophenyl)-1H-pyrazole

4-fluoroaniline

Rh(CO)(P(C₆H₅)3)2((FC₆H₄)2N₃H)⁽¹⁺⁾*BF₄^(1-)=[Rh(CO)(P(C₆H₅)3)2((FC₆H₄)2N₃H)][BF₄]