(Sp)-1-[(1R)-(1-(3H-isobenzofuran-1-ylideneamino)-ethyl)]-2-(diphenylphosphino)-ferrocene

Base Information

• Chemical Name: (Sp)-1-[(1R)-(1-(3H-isobenzofuran-1-ylideneamino)-ethyl)]-2-(diphenylphosphino)-ferrocene
• CAS No.: 1243536-88-0
• Molecular Formula: C₃₂H₂₈FeNOP
• Molecular Weight: 529.401

Synonyms:(Sp)-1-[(1R)-(1-(3H-isobenzofuran-1-ylideneamino)-ethyl)]-2-(diphenylphosphino)-ferrocene

Chemical Property of (Sp)-1-[(1R)-(1-(3H-isobenzofuran-1-ylideneamino)-ethyl)]-2-(diphenylphosphino)-ferrocene

Chemical Property:

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Technology Process of (Sp)-1-[(1R)-(1-(3H-isobenzofuran-1-ylideneamino)-ethyl)]-2-(diphenylphosphino)-ferrocene

There total 1 articles about (Sp)-1-[(1R)-(1-(3H-isobenzofuran-1-ylideneamino)-ethyl)]-2-(diphenylphosphino)-ferrocene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1,3-dihydro-1-iminoisobenzofuran hydrochloride (1195988-94-3) + (Sp)-1-[(1R)-(1-aminoethyl)]-2-(diphenylphosphino)-ferrocene (1384443-98-4,172041-83-7,406681-19-4,607389-84-4) → (Sp)-1-[(1R)-(1-(3H-isobenzofuran-1-ylideneamino)-ethyl)]-2-(diphenylphosphino)-ferrocene (1243536-88-0)

Guidance literature:

With triethylamine; In dichloromethane; for 48h; Cooling with ice; Reflux;

Reference yield: 91.0%

bis(1,5-cyclooctadiene)diiridium(I) dichloride (12112-67-3) + (Sp)-1-[(1R)-(1-(3H-isobenzofuran-1-ylideneamino)-ethyl)]-2-(diphenylphosphino)-ferrocene (1243536-88-0) + sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate (79060-88-1) → C32H12BF24(1-)*C40H40FeIrNOP(1+) (1251832-04-8)

Guidance literature:

In dichloromethane; for 2h; Inert atmosphere; Reflux;

upstream raw materials:

1,3-dihydro-1-iminoisobenzofuran hydrochloride

(Sp)-1-[(1R)-(1-aminoethyl)]-2-(diphenylphosphino)-ferrocene

Downstream raw materials:

C₃₂H₁₂BF₂₄^(1-)*C₄₀H₄₀FeIrNOP⁽¹⁺⁾

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