1-{6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridin-3-yl}-1-methylethylamine

Base Information

Chemical Name:1-{6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridin-3-yl}-1-methylethylamine
CAS No.:1057677-39-0
Molecular Formula:C₂₇H₃₀N₆
Molecular Weight:438.575
Hs Code.:

Synonyms:1-{6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridin-3-yl}-1-methylethylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-{6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridin-3-yl}-1-methylethylamine

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Technology Process of 1-{6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridin-3-yl}-1-methylethylamine

There total 2 articles about 1-{6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridin-3-yl}-1-methylethylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.2%

: 1057676-76-2
6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]nicotinonitrile

: 94616-84-9
dichloromethylcerium

: 1057677-39-0
1-{6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridin-3-yl}-1-methylethylamine

Guidance literature:: In tetrahydrofuran; at 20 ℃;

Reference yield: 37.0%

: 1057676-76-2
6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]nicotinonitrile

: 75-16-1
methylmagnesium bromide

: 1057677-39-0
1-{6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridin-3-yl}-1-methylethylamine

Guidance literature:: methylmagnesium bromide; With cerium(III) chloride; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]nicotinonitrile; In tetrahydrofuran; at 20 ℃; Inert atmosphere;
DOI:10.1021/jm900309j

Reference yield: 74.1%

: 1057677-39-0
1-{6-[4-(4-benzylphthalazin-1-yl)piperazin-1-yl]pyridin-3-yl}-1-methylethylamine

: 1057677-40-3
N-(2-(6-(4-(4-benzylphthalazin-1-yl)piperazin-1-yl)pyridin-3-yl)propan-2-yl)-2-methoxyacetamide

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; dmap; In dichloromethane; at 20 ℃; for 16h;