C₃₇H₅₄O₅

Base Information

• Chemical Name: C₃₇H₅₄O₅
• CAS No.: 1184938-08-6
• Molecular Formula: C₃₇H₅₄O₅
• Molecular Weight: 578.833
• Mol file: 1184938-08-6.mol

Synonyms:C₃₇H₅₄O₅

Chemical Property of C₃₇H₅₄O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₇H₅₄O₅

There total 3 articles about C₃₇H₅₄O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-decyloxy-benzoic acid ethyl ester (154845-74-6) + acetone (67-64-1) → C37H54O5 (1184938-08-6)

Guidance literature:

With hydrogenchloride; sodium hydride; In 1,2-dimethoxyethane; mineral oil; for 24h; Inert atmosphere; Reflux;

DOI:10.1016/j.dyepig.2015.10.029

Reference yield:

methyl 4-decyloxybenzoate (62443-10-1) + acetone (67-64-1) → C37H54O5 (1184938-08-6)

Guidance literature:

With sodium hydride; In 1,2-dimethoxyethane; for 48h; Reflux;

DOI:10.1016/j.tet.2008.11.080

Reference yield:

Ethyl 4-hydroxybenzoate (120-47-8) → C37H54O5 (1184938-08-6)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium iodide; potassium carbonate / acetone / Reflux

2: sodium hydride; hydrogenchloride / 1,2-dimethoxyethane; mineral oil / 24 h / Inert atmosphere; Reflux

With hydrogenchloride; sodium hydride; potassium carbonate; potassium iodide; In 1,2-dimethoxyethane; acetone; mineral oil; 1: |Williamson Ether Synthesis / 2: |Claisen Condensation;

DOI:10.1016/j.dyepig.2015.10.029

upstream raw materials:

methyl 4-decyloxybenzoate

acetone

Ethyl 4-hydroxybenzoate

4-decyloxy-benzoic acid ethyl ester

Downstream raw materials:

1-(4-decyloxyphenyl)-2-(3-(4-decyloxyphenyl)-1H-pyrazol-5-yl)ethanone

Refernces

• 1、 Chou, Shih-Yu,Chen, Chun-Jung,Tsai, Shao-Ling,Sheu, Hwo-Shuenn,Lee, Gene-Hsiang,Lai, Chung K.. "Columnar metallomesogens derived from unsymmetrical pyrazoles". scheme or table. p. 1130 - 1139. Retrieved 2009/04/10.