(S)-2-benzyloxycarbonylamino-2-(thiophen-2-yl)-acetonitrile

Base Information Edit

Chemical Name:(S)-2-benzyloxycarbonylamino-2-(thiophen-2-yl)-acetonitrile
CAS No.:1355742-75-4
Molecular Formula:C₁₄H₁₂N₂O₂S
Molecular Weight:272.327
Hs Code.:
Mol file:1355742-75-4.mol

Synonyms:(S)-2-benzyloxycarbonylamino-2-(thiophen-2-yl)-acetonitrile

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Chemical Property of (S)-2-benzyloxycarbonylamino-2-(thiophen-2-yl)-acetonitrile Edit

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Technology Process of (S)-2-benzyloxycarbonylamino-2-(thiophen-2-yl)-acetonitrile

There total 1 articles about (S)-2-benzyloxycarbonylamino-2-(thiophen-2-yl)-acetonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 7677-24-9
trimethylsilyl cyanide

: 502929-72-8
[1-Thiophen-2-yl-meth-(E)-ylidene]-carbamic acid benzyl ester

: 1355742-75-4
(S)-2-benzyloxycarbonylamino-2-(thiophen-2-yl)-acetonitrile

Guidance literature:: trimethylsilyl cyanide; With methanol; [Ru{(S)-phgly}2{(S)-binap}]; at 0 ℃; for 0.25h; Inert atmosphere;

[1-Thiophen-2-yl-meth-(E)-ylidene]-carbamic acid benzyl ester; In tert-butyl methyl ether; at 0 ℃; for 0.25h; Inert atmosphere;

With lithium phenolate; In tetrahydrofuran; tert-butyl methyl ether; at 0 ℃; for 0.5h; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ol203408w