C₆H₄(P(C₆H₅)2)O(BO(OC(CH₃)2)2)

Base Information

Chemical Name:C₆H₄(P(C₆H₅)2)O(BO(OC(CH₃)2)2)
CAS No.:1250439-05-4
Molecular Formula:C₂₄H₂₆BO₄P
Molecular Weight:420.253
Hs Code.:

C<sub>6</sub>H<sub>4</sub>(P(C<sub>6</sub>H<sub>5</sub>)2)O(BO(OC(CH<sub>3</sub>)2)2)

Synonyms:C₆H₄(P(C₆H₅)2)O(BO(OC(CH₃)2)2)

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Chemical Property of C₆H₄(P(C₆H₅)2)O(BO(OC(CH₃)2)2)

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Technology Process of C₆H₄(P(C₆H₅)2)O(BO(OC(CH₃)2)2)

There total 2 articles about C₆H₄(P(C₆H₅)2)O(BO(OC(CH₃)2)2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1250258-94-6
[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenyl]diphenylphosphine

: 1250439-05-4
C₆H₄(P(C₆H₅)2)O(BO(OC(CH₃)2)2)

Guidance literature:: With oxygen; 5,15,10,20-tetraphenylporphyrin; In toluene; at 20 ℃; for 3h; under 760.051 Torr; UV-irradiation;
DOI:10.1002/anie.201000520

Reference yield: 48.0%

: 1250258-94-6
[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenyl]diphenylphosphine

: 80937-33-3
oxygen

: 1250439-05-4
C₆H₄(P(C₆H₅)2)O(BO(OC(CH₃)2)2)

Guidance literature:: With tetraphenylporphyrine; In toluene; Irradiation (UV/VIS); Schlenk technique; soln. of phosphine-borane compound containing tetraphenylporphyrin irradiated with halogen lamp under dried O2, room temp., 3h; toluene removed (vac.), residue purified by crystallization in diethyl ether; conversion monitored with (31)P NMR;
DOI:10.1002/anie.201000520

Reference yield: 100.0%

: 1250258-94-6
[2-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)phenyl]diphenylphosphine

: 1250439-05-4
C₆H₄(P(C₆H₅)2)O(BO(OC(CH₃)2)2)

: 1250439-08-7
C₆H₄(PO(C₆H₅)2)(B(OC(CH₃)2)2)

Guidance literature:: In toluene; Schlenk technique, heated overnight at 100 °C; recrystd. in diethyl ether/pentane; detd. by XRD, NMR;
DOI:10.1002/anie.201000520