Acetic acid (2S,3S)-3-[(1-amino-cyclohexanecarbonyl)-amino]-4-oxo-azetidin-2-yl ester

Base Information

• Chemical Name: Acetic acid (2S,3S)-3-[(1-amino-cyclohexanecarbonyl)-amino]-4-oxo-azetidin-2-yl ester
• CAS No.: 874212-46-1
• Molecular Formula: C₁₂H₁₉N₃O₄
• Molecular Weight: 269.301

Synonyms:Acetic acid (2S,3S)-3-[(1-amino-cyclohexanecarbonyl)-amino]-4-oxo-azetidin-2-yl ester

Chemical Property of Acetic acid (2S,3S)-3-[(1-amino-cyclohexanecarbonyl)-amino]-4-oxo-azetidin-2-yl ester

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Technology Process of Acetic acid (2S,3S)-3-[(1-amino-cyclohexanecarbonyl)-amino]-4-oxo-azetidin-2-yl ester

There total 1 articles about Acetic acid (2S,3S)-3-[(1-amino-cyclohexanecarbonyl)-amino]-4-oxo-azetidin-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Acetic acid (2S,3S)-3-[(1-benzyloxycarbonylamino-cyclohexanecarbonyl)-amino]-4-oxo-azetidin-2-yl ester (455253-68-6) → Acetic acid (2S,3S)-3-[(1-amino-cyclohexanecarbonyl)-amino]-4-oxo-azetidin-2-yl ester (874212-46-1)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; for 8h; under 2585.74 Torr;

DOI:10.1016/j.bmcl.2004.12.088

Reference yield:

4-(methylthio)benzoic acid (13205-48-6,562836-64-0) + Acetic acid (2S,3S)-3-[(1-amino-cyclohexanecarbonyl)-amino]-4-oxo-azetidin-2-yl ester (874212-46-1) → Acetic acid (2S,3S)-3-{[1-(4-methylsulfanyl-benzoylamino)-cyclohexanecarbonyl]-amino}-4-oxo-azetidin-2-yl ester

Guidance literature:

With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In ethyl acetate; N,N-dimethyl-formamide; at 20 ℃; for 18h;

DOI:10.1016/j.bmcl.2004.12.088

Reference yield:

p-N,N-dimethylaminobenzoic acid (619-84-1) + Acetic acid (2S,3S)-3-[(1-amino-cyclohexanecarbonyl)-amino]-4-oxo-azetidin-2-yl ester (874212-46-1) → Acetic acid (2S,3S)-3-{[1-(4-dimethylamino-benzoylamino)-cyclohexanecarbonyl]-amino}-4-oxo-azetidin-2-yl ester

Guidance literature:

With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In ethyl acetate; N,N-dimethyl-formamide; at 20 ℃; for 18h;

DOI:10.1016/j.bmcl.2004.12.088

upstream raw materials:

Acetic acid (2S,3S)-3-[(1-benzyloxycarbonylamino-cyclohexanecarbonyl)-amino]-4-oxo-azetidin-2-yl ester

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