carbonic acid 2-(14-allyloxyimino-4-ethyl-11-methoxy-2,2,3a,7,9,11,13,15-octamethyl-6,8-dioxo-dodecahydro-1,3,5-trioxa-cyclopentacyclotetradecen-10-yloxy)-4-(benzyloxycarbonyl-methyl-amino)-6-methyl-tetrahydro-pyran-3-yl ester benzyl ester

Base Information

Chemical Name:carbonic acid 2-(14-allyloxyimino-4-ethyl-11-methoxy-2,2,3a,7,9,11,13,15-octamethyl-6,8-dioxo-dodecahydro-1,3,5-trioxa-cyclopentacyclotetradecen-10-yloxy)-4-(benzyloxycarbonyl-methyl-amino)-6-methyl-tetrahydro-pyran-3-yl ester benzyl ester
CAS No.:869317-78-2
Molecular Formula:C₅₁H₇₂N₂O₁₄
Molecular Weight:937.138
Hs Code.:

carbonic acid 2-(14-allyloxyimino-4-ethyl-11-methoxy-2,2,3a,7,9,11,13,15-octamethyl-6,8-dioxo-dodecahydro-1,3,5-trioxa-cyclopentacyclotetradecen-10-yloxy)-4-(benzyloxycarbonyl-methyl-amino)-6-methyl-tetrahydro-pyran-3-yl ester benzyl ester

Synonyms:carbonic acid 2-(14-allyloxyimino-4-ethyl-11-methoxy-2,2,3a,7,9,11,13,15-octamethyl-6,8-dioxo-dodecahydro-1,3,5-trioxa-cyclopentacyclotetradecen-10-yloxy)-4-(benzyloxycarbonyl-methyl-amino)-6-methyl-tetrahydro-pyran-3-yl ester benzyl ester

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Chemical Property of carbonic acid 2-(14-allyloxyimino-4-ethyl-11-methoxy-2,2,3a,7,9,11,13,15-octamethyl-6,8-dioxo-dodecahydro-1,3,5-trioxa-cyclopentacyclotetradecen-10-yloxy)-4-(benzyloxycarbonyl-methyl-amino)-6-methyl-tetrahydro-pyran-3-yl ester benzyl ester

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Technology Process of carbonic acid 2-(14-allyloxyimino-4-ethyl-11-methoxy-2,2,3a,7,9,11,13,15-octamethyl-6,8-dioxo-dodecahydro-1,3,5-trioxa-cyclopentacyclotetradecen-10-yloxy)-4-(benzyloxycarbonyl-methyl-amino)-6-methyl-tetrahydro-pyran-3-yl ester benzyl ester

There total 3 articles about carbonic acid 2-(14-allyloxyimino-4-ethyl-11-methoxy-2,2,3a,7,9,11,13,15-octamethyl-6,8-dioxo-dodecahydro-1,3,5-trioxa-cyclopentacyclotetradecen-10-yloxy)-4-(benzyloxycarbonyl-methyl-amino)-6-methyl-tetrahydro-pyran-3-yl ester benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 860476-67-1
carbonic acid 2-(10-allyloxyimino-14-ethyl-12,13-dihydroxy-7-methoxy-3,5,7,9,11,13-hexamethyl-2,4-dioxo-oxacyclotetradec-6-yloxy)-4-(benzyloxycarbonyl-methyl-amino)-6-methyl-tetrahydro-pyran-3-yl ester benzyl ester

: 77-76-9
2,2-dimethoxy-propane

: 869317-78-2
carbonic acid 2-(14-allyloxyimino-4-ethyl-11-methoxy-2,2,3a,7,9,11,13,15-octamethyl-6,8-dioxo-dodecahydro-1,3,5-trioxa-cyclopentacyclotetradecen-10-yloxy)-4-(benzyloxycarbonyl-methyl-amino)-6-methyl-tetrahydro-pyran-3-yl ester benzyl ester

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 72h; Heating;
DOI:10.1016/j.bmc.2005.06.003

Reference yield:

: C₅₆H₈₄N₂O₁₇

: 869317-78-2
carbonic acid 2-(14-allyloxyimino-4-ethyl-11-methoxy-2,2,3a,7,9,11,13,15-octamethyl-6,8-dioxo-dodecahydro-1,3,5-trioxa-cyclopentacyclotetradecen-10-yloxy)-4-(benzyloxycarbonyl-methyl-amino)-6-methyl-tetrahydro-pyran-3-yl ester benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / hydrochloric acid / tetrahydrofuran / 1.5 h / 20 °C

2: 85 percent / DMSO; (CF₃CO)2O; Et₃N / CH₂Cl₂ / 1 h / -78 °C

3: 86 percent / p-TsOH*H₂O / toluene / 72 h / Heating

With hydrogenchloride; toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1016/j.bmc.2005.06.003

Reference yield:

: 860476-66-0
carbonic acid 2-(10-allyloxyimino-14-ethyl-4,12,13-trihydroxy-7-methoxy-3,5,7,9,11,13-hexamethyl-2-oxo-oxacyclotetradec-6-yloxy)-4-(benzyloxycarbonyl-methyl-amino)-6-methyl-tetrahydro-pyran-3-yl ester benzyl ester

: 869317-78-2
carbonic acid 2-(14-allyloxyimino-4-ethyl-11-methoxy-2,2,3a,7,9,11,13,15-octamethyl-6,8-dioxo-dodecahydro-1,3,5-trioxa-cyclopentacyclotetradecen-10-yloxy)-4-(benzyloxycarbonyl-methyl-amino)-6-methyl-tetrahydro-pyran-3-yl ester benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / DMSO; (CF₃CO)2O; Et₃N / CH₂Cl₂ / 1 h / -78 °C

2: 86 percent / p-TsOH*H₂O / toluene / 72 h / Heating

With toluene-4-sulfonic acid; dimethyl sulfoxide; triethylamine; trifluoroacetic anhydride; In dichloromethane; toluene;
DOI:10.1016/j.bmc.2005.06.003