2-(2-benzenesulfonylethyl)-1-ethenylcyclohexanol

Base Information

• Chemical Name: 2-(2-benzenesulfonylethyl)-1-ethenylcyclohexanol
• CAS No.: 1234563-94-0
• Molecular Formula: C₁₆H₂₂O₃S
• Molecular Weight: 294.415
• Mol file: 1234563-94-0.mol

Synonyms:2-(2-benzenesulfonylethyl)-1-ethenylcyclohexanol

Chemical Property of 2-(2-benzenesulfonylethyl)-1-ethenylcyclohexanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of 2-(2-benzenesulfonylethyl)-1-ethenylcyclohexanol

There total 1 articles about 2-(2-benzenesulfonylethyl)-1-ethenylcyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

2-<2-(phenylsulfonyl)ethyl>cyclohexanone (6517-32-4) + vinyl magnesium bromide (1826-67-1) → 2-(2-benzenesulfonylethyl)-1-ethenylcyclohexanol (1234563-94-0)

Guidance literature:

2-<2-(phenylsulfonyl)ethyl>cyclohexanone; vinyl magnesium bromide; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;

With ammonium chloride; In tetrahydrofuran; diethyl ether; water; Inert atmosphere;

DOI:10.1016/j.tet.2010.03.107

Reference yield:

2-(2-benzenesulfonylethyl)-1-ethenylcyclohexanol (1234563-94-0) → (E)-1-(2-benzenesulfonylethyl)-2-(2-bromoethylidene)cyclohexane (1234563-95-1)

Guidance literature:

With pyridine; phosphorus tribromide; Darkness; Inert atmosphere;

DOI:10.1016/j.tet.2010.03.107

upstream raw materials:

2-<2-(phenylsulfonyl)ethyl>cyclohexanone

vinyl magnesium bromide

Downstream raw materials:

(E)-1-(2-benzenesulfonylethyl)-2-(2-bromoethylidene)cyclohexane