5-(1-Boc-2-indolyl)-3-Methoxypyrrole-2-carboxaldehyde, 97%

Base Information

Chemical Name:5-(1-Boc-2-indolyl)-3-Methoxypyrrole-2-carboxaldehyde, 97%
CAS No.:1033391-26-2
Molecular Formula:C₁₉H₂₀N₂O₄
Molecular Weight:340.379
Hs Code.:
Mol file:1033391-26-2.mol

Synonyms:tert-butyl 2-(5-formyl-4-methoxy-1H-pyrrol-2-yl)-1H-indole-1-carboxylate

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Chemical Property of 5-(1-Boc-2-indolyl)-3-Methoxypyrrole-2-carboxaldehyde, 97%

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Technology Process of 5-(1-Boc-2-indolyl)-3-Methoxypyrrole-2-carboxaldehyde, 97%

There total 4 articles about 5-(1-Boc-2-indolyl)-3-Methoxypyrrole-2-carboxaldehyde, 97% which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 960509-42-6
N-((5-bromo-3-methoxy-2H-pyrrol-2-ylidene)methyl)-N-ethylethanamine

: 213318-44-6
N-Boc-indole-2-boronic acid

: 803712-70-1
tert-butyl 2-(5-formyl-4-methoxy-1H-pyrrol-2-yl)-1H-indole-1-carboxylate

: 1033391-26-2
tert-butyl 2-(5-formyl-4-methoxy-1H-pyrrol-2-yl)-1H-indole-1-carboxylate

Guidance literature:: With sodium carbonate; palladium diacetate; triphenylphosphine; In 1,4-dioxane; water; toluene; at 98 ℃;
DOI:10.1039/b719353j

Reference yield: 62.5%

: 803712-71-2
N-((5-bromo-3-methoxy-2H-pyrrol-2-ylidene)-methyl)-N-ethylethanamine

: 213318-44-6
N-Boc-indole-2-boronic acid

: 1033391-26-2
tert-butyl 2-(5-formyl-4-methoxy-1H-pyrrol-2-yl)-1H-indole-1-carboxylate

Guidance literature:: N-((5-bromo-3-methoxy-2H-pyrrol-2-ylidene)methyl)-N-ethylethanamine; N-Boc-indole-2-boronic acid; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,4-dioxane; water; Schlenk technique; Inert atmosphere; Heating;

With hydrogenchloride; water; In 1,4-dioxane; pH=7; Cooling with ice;
DOI:10.1021/acsmedchemlett.9b00304

Reference yield:

: 1413942-20-7
C₁₀H₁₆N₂O₂

: 213318-44-6
N-Boc-indole-2-boronic acid

: 1033391-26-2
tert-butyl 2-(5-formyl-4-methoxy-1H-pyrrol-2-yl)-1H-indole-1-carboxylate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; In 1,4-dioxane; water; toluene; at 100 ℃; for 1.5h; Inert atmosphere;
DOI:10.1016/j.ejmech.2012.08.024