6-aminopenicillanic acid trichloroethyl ester p-toluenesulfonate salt

Base Information

Chemical Name:6-aminopenicillanic acid trichloroethyl ester p-toluenesulfonate salt
CAS No.:30246-35-6
Molecular Formula:C₇H₈O₃S*C₁₀H₁₃Cl₃N₂O₃S
Molecular Weight:519.855
Hs Code.:

Synonyms:6-aminopenicillanic acid trichloroethyl ester p-toluenesulfonate salt

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Chemical Property of 6-aminopenicillanic acid trichloroethyl ester p-toluenesulfonate salt

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Technology Process of 6-aminopenicillanic acid trichloroethyl ester p-toluenesulfonate salt

There total 3 articles about 6-aminopenicillanic acid trichloroethyl ester p-toluenesulfonate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 87106-46-5
(2S,5R,6R)-6-((Z)-2-Methoxycarbonyl-1-methyl-vinylamino)-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid 2,2,2-trichloro-ethyl ester

: 104-15-4
toluene-4-sulfonic acid

: 30246-35-6
6-aminopenicillanic acid trichloroethyl ester p-toluenesulfonate salt

Guidance literature:: In acetone; for 0.166667h; Ambient temperature;
DOI:10.1055/s-1983-30419

Reference yield:

: 551-16-6
6-Aminopenicillanic Acid

: 30246-35-6
6-aminopenicillanic acid trichloroethyl ester p-toluenesulfonate salt

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) N(C₂H₅)3 / 1.) CH₂Cl₂, room temp., 2.) 3 h, room temp.

2: 55 percent / 4-(dimethylamino)-pyridine, 1-ethyl-3<(3-dimethylamino)-propyl>carbodiimide / CH₂Cl₂ / 1.) 2 h, 0 - 10 degC, 2.) 2 h, room temp.

3: 83 percent / acetone / 0.17 h / Ambient temperature

With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In dichloromethane; acetone;
DOI:10.1055/s-1983-30419

Reference yield:

: 87106-41-0
(2S,5R,6R)-6-((Z)-2-Methoxycarbonyl-1-methyl-vinylamino)-3,3-dimethyl-7-oxo-4-thia-1-aza-bicyclo[3.2.0]heptane-2-carboxylic acid; compound with triethyl-amine

: 30246-35-6
6-aminopenicillanic acid trichloroethyl ester p-toluenesulfonate salt

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / 4-(dimethylamino)-pyridine, 1-ethyl-3<(3-dimethylamino)-propyl>carbodiimide / CH₂Cl₂ / 1.) 2 h, 0 - 10 degC, 2.) 2 h, room temp.

2: 83 percent / acetone / 0.17 h / Ambient temperature

With dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; acetone;
DOI:10.1055/s-1983-30419