6-(4-methoxybenzyloxy)-hex-2-enal

Base Information

Chemical Name:6-(4-methoxybenzyloxy)-hex-2-enal
CAS No.:869226-87-9
Molecular Formula:C₁₄H₁₈O₃
Molecular Weight:234.295
Hs Code.:

Synonyms:6-(4-methoxybenzyloxy)-hex-2-enal

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Chemical Property of 6-(4-methoxybenzyloxy)-hex-2-enal

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Technology Process of 6-(4-methoxybenzyloxy)-hex-2-enal

There total 1 articles about 6-(4-methoxybenzyloxy)-hex-2-enal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 197219-35-5
6-[(4-methoxyphenyl)methoxy]-(E)-2-hexen-1-ol

: 869226-87-9
6-(4-methoxybenzyloxy)-hex-2-enal

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 - 20 ℃;
DOI:10.1021/jo051318i

Reference yield: 67.0%

: 869226-87-9
6-(4-methoxybenzyloxy)-hex-2-enal

: 105-45-3
acetoacetic acid methyl ester

: 869226-88-0
5-hydroxy-10-(4-methoxybenzyloxy)-3-oxo-dec-6-enoic acid methyl ester

Guidance literature:: acetoacetic acid methyl ester; With n-butyllithium; sodium hydride; In tetrahydrofuran; hexane; at 0 ℃;

6-(4-methoxybenzyloxy)-hex-2-enal; In tetrahydrofuran; hexane; at -78 ℃; for 0.333333h;
DOI:10.1021/jo051318i

Reference yield:

: 869226-87-9
6-(4-methoxybenzyloxy)-hex-2-enal

: 2-[5-(4-methoxybenzyloxy)-pent-1-enyl]-6-vinyl-3,4-dihydro-2H-pyran-4-ol

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride; n-butyllithium / tetrahydrofuran; hexane / 0 °C

1.2: 67 percent / tetrahydrofuran; hexane / 0.33 h / -78 °C

2.1: tetramethylammonium borohydride; acetic acid / acetonitrile / 15 h / -25 °C

3.1: 407 mg / trifluoroacetic acid / CH₂Cl₂ / 15 h / 20 °C

4.1: 80 percent / triethylamine; 4-(dimethylamino)pyridine / tetrahydrofuran / 0.5 h

5.1: tetrahydrofuran / 0.5 h / -78 °C

6.1: thionyl chloride; 4-(dimethylamino)pyridine / CH₂Cl₂ / 30 h

7.1: 392 mg / tetrabutylammonium fluoride / tetrahydrofuran / 0.5 h

With dmap; n-butyllithium; thionyl chloride; tetramethylammonium borohydride; tetrabutyl ammonium fluoride; sodium hydride; acetic acid; triethylamine; trifluoroacetic acid; In tetrahydrofuran; hexane; dichloromethane; acetonitrile;
DOI:10.1021/jo051318i