2-amino-N-(2-oxoindol-3-yl)benzohydrazide

Base Information

• Chemical Name: 2-amino-N-(2-oxoindol-3-yl)benzohydrazide
• CAS No.: 5061-17-6
• Molecular Formula: C₁₅H₁₂N₄O₂
• Molecular Weight: 280.286
• Mol file: 5061-17-6.mol

Synonyms:

Chemical Property of 2-amino-N-(2-oxoindol-3-yl)benzohydrazide

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-amino-N-(2-oxoindol-3-yl)benzohydrazide

There total 1 articles about 2-amino-N-(2-oxoindol-3-yl)benzohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

indole-2,3-dione (91-56-5,1186480-61-4,84788-92-1) + anthranilic acid hydrazide (1904-58-1) → 1-isatin-3-o-aminobenzoylhydrazone (5061-17-6)

Guidance literature:

In methanol; for 3h;

DOI:10.1002/aoc.3252

Reference yield: 80.0%

1-isatin-3-o-aminobenzoylhydrazone (5061-17-6) + copper diacetate (142-71-2) → Cu(C6H4NHCOCN2COC6H4NH2)(CH3COO)(H2O)

Guidance literature:

In ethanol; equimolar amts. of educts in aq. EtOH were refluxed on water bath for 1h; elem. anal.;

Reference yield: 76.0%

1-isatin-3-o-aminobenzoylhydrazone (5061-17-6) + nickel diacetate (373-02-4,14998-37-9,33025-09-1,94044-50-5,98268-31-6) → Ni(C6H4NHCOCN2COC6H4NH2)(CH3COO)(H2O)*3H2O

Guidance literature:

With sodium acetate; In ethanol; equimolar amts. of educts in aq. EtOH in the presence of CH3COONa were refluxed on water bath for 3 h; elem. anal.;

upstream raw materials:

indole-2,3-dione

anthranilic acid hydrazide

Downstream raw materials:

dichloro(1-isatin-3-o-aminobenzoylhydrazone)cadmium

dichloro(1-isatin-3-o-aminobenzoylhydrazone)zinc(II)

Refernces