[3,5-dichloro-4-(6-chloro-5-isopropylpyridazin-3-yloxy)phenyl]acetic acid

Base Information

Chemical Name:[3,5-dichloro-4-(6-chloro-5-isopropylpyridazin-3-yloxy)phenyl]acetic acid
CAS No.:920509-22-4
Molecular Formula:C₁₅H₁₃Cl₃N₂O₃
Molecular Weight:375.639
Hs Code.:

Synonyms:[3,5-dichloro-4-(6-chloro-5-isopropylpyridazin-3-yloxy)phenyl]acetic acid

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Chemical Property of [3,5-dichloro-4-(6-chloro-5-isopropylpyridazin-3-yloxy)phenyl]acetic acid

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Technology Process of [3,5-dichloro-4-(6-chloro-5-isopropylpyridazin-3-yloxy)phenyl]acetic acid

There total 4 articles about [3,5-dichloro-4-(6-chloro-5-isopropylpyridazin-3-yloxy)phenyl]acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 920509-21-3
2-[3,5-dichloro-4-(6-chloro-5-isopropylpyridazin-3-yloxy)phenyl]ethanol

: 920509-22-4
[3,5-dichloro-4-(6-chloro-5-isopropylpyridazin-3-yloxy)phenyl]acetic acid

Guidance literature:: With Jones reagent; In acetone; at -4 - 0 ℃; for 1h;

Reference yield:

: 115150-58-8
2-(3,5-dichloro-4-hydroxyphenyl)ethanol

: 920509-22-4
[3,5-dichloro-4-(6-chloro-5-isopropylpyridazin-3-yloxy)phenyl]acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / N,N-dimethyl acetamide / 24 h / 20 - 135 °C

2: Jones reagent / acetone / 1 h / -3 - 0 °C

With Jones reagent; potassium tert-butylate; In N,N-dimethyl acetamide; acetone;
DOI:10.1021/jm4019299

Reference yield:

: 14199-15-6
Methyl 4-hydroxyphenylacetate

: 920509-22-4
[3,5-dichloro-4-(6-chloro-5-isopropylpyridazin-3-yloxy)phenyl]acetic acid

Guidance literature:: Multi-step reaction with 4 steps

1: diisobutylamine; sulfuryl dichloride / toluene / 1.5 h / 20 - 70 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 0.08 h / -10 °C / Inert atmosphere

3: potassium tert-butylate / N,N-dimethyl acetamide / 24 h / 20 - 135 °C

4: Jones reagent / acetone / 1 h / -3 - 0 °C

With lithium aluminium tetrahydride; Jones reagent; diisobutylamine; sulfuryl dichloride; potassium tert-butylate; In tetrahydrofuran; N,N-dimethyl acetamide; acetone; toluene;
DOI:10.1021/jm4019299