2-[3,5-dichloro-4-(6-chloro-5-isopropylpyridazin-3-yloxy)phenyl]ethanol

Base Information

Chemical Name:2-[3,5-dichloro-4-(6-chloro-5-isopropylpyridazin-3-yloxy)phenyl]ethanol
CAS No.:920509-21-3
Molecular Formula:C₁₅H₁₅Cl₃N₂O₂
Molecular Weight:361.655
Hs Code.:

Synonyms:2-[3,5-dichloro-4-(6-chloro-5-isopropylpyridazin-3-yloxy)phenyl]ethanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[3,5-dichloro-4-(6-chloro-5-isopropylpyridazin-3-yloxy)phenyl]ethanol

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Technology Process of 2-[3,5-dichloro-4-(6-chloro-5-isopropylpyridazin-3-yloxy)phenyl]ethanol

There total 4 articles about 2-[3,5-dichloro-4-(6-chloro-5-isopropylpyridazin-3-yloxy)phenyl]ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 107228-51-3
3,6-dichloro-4-isopropyl-1,2-dihydropyridazine

: 920509-21-3
2-[3,5-dichloro-4-(6-chloro-5-isopropylpyridazin-3-yloxy)phenyl]ethanol

Guidance literature:: 2-(3,5-dichloro-4-hydroxyphenyl)ethanol; With potassium tert-butylate; In N,N-dimethyl acetamide; at 20 - 100 ℃;

3,6-dichloro-4-isopropyl-1,2-dihydropyridazine; In N,N-dimethyl acetamide; at 135 ℃; for 24h;

Reference yield: 44.0%

: 107228-51-3
3,6-dichloro-4-isopropyl-1,2-dihydropyridazine

: 115150-58-8
2-(3,5-dichloro-4-hydroxyphenyl)ethanol

: 920509-21-3
2-[3,5-dichloro-4-(6-chloro-5-isopropylpyridazin-3-yloxy)phenyl]ethanol

Guidance literature:: With potassium tert-butylate; In N,N-dimethyl acetamide; at 20 - 135 ℃; for 24h;
DOI:10.1021/jm4019299

Reference yield:

: 14199-15-6
Methyl 4-hydroxyphenylacetate

: 920509-21-3
2-[3,5-dichloro-4-(6-chloro-5-isopropylpyridazin-3-yloxy)phenyl]ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: diisobutylamine; sulfuryl dichloride / toluene / 1.5 h / 20 - 70 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 0.08 h / -10 °C / Inert atmosphere

3: potassium tert-butylate / N,N-dimethyl acetamide / 24 h / 20 - 135 °C

With lithium aluminium tetrahydride; diisobutylamine; sulfuryl dichloride; potassium tert-butylate; In tetrahydrofuran; N,N-dimethyl acetamide; toluene;
DOI:10.1021/jm4019299