1,4-Bis(4-methylbenzoyl)benzene

Base Information

Chemical Name:1,4-Bis(4-methylbenzoyl)benzene
CAS No.:61565-13-7
Molecular Formula:C22H18O2
Molecular Weight:314.384
Hs Code.:
NSC Number:78842
DSSTox Substance ID:DTXSID90977156
Nikkaji Number:J1.518.411F
Wikidata:Q82962238

Synonyms:61565-13-7;Benzene, p-di-p-toluyl-;NIOSH/PC4974000;1,4-Phenylenebis((4-methylphenyl)methanone);PC49740000;Methanone, 1,4-phenylenebis((4-methylphenyl)-;NSC78842;NCIOpen2_008862;Oprea1_034946;Oprea1_565838;SCHEMBL822185;DTXSID90977156;PATGGWXAIDKGEG-UHFFFAOYSA-N;1,4-di(4'-methylbenzoyl)benzene;NSC-78842;AKOS000747304;(1,4-Phenylene)bis[(4-methylphenyl)methanone];Methanone, 1,1'-(1,4-phenylene)bis[1-(4-methylphenyl)-

Suppliers and Price of 1,4-Bis(4-methylbenzoyl)benzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 1,4-Bis(4-methylbenzoyl)benzene

Chemical Property:

Vapor Pressure:5.11E-10mmHg at 25°C
Boiling Point:497.1°Cat760mmHg
Flash Point:183.9°C
Density:1.129g/cm³
XLogP3:5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:314.130679813
Heavy Atom Count:24
Complexity:389

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)C(=O)C2=CC=C(C=C2)C(=O)C3=CC=C(C=C3)C

Technology Process of 1,4-Bis(4-methylbenzoyl)benzene

There total 12 articles about 1,4-Bis(4-methylbenzoyl)benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 201230-82-2
carbon monoxide

: 624-38-4,1032416-46-8
para-diiodobenzene

: 5720-05-8
4-methylphenylboronic acid

: 61565-13-7
1,4-phenylenebis[(4-methylphenyl)methanone]

Guidance literature:: With potassium carbonate; bis-triphenylphosphine-palladium(II) chloride; In various solvent(s); at 80 ℃; for 5h;
DOI:10.1016/S0040-4039(00)60409-4

Reference yield: 77.0%

: 100-20-9
terephthaloyl chloride

: 108-88-3,15644-74-3,16713-13-6
toluene

: 61565-13-7
1,4-phenylenebis[(4-methylphenyl)methanone]

Guidance literature:: With aluminum (III) chloride; In 1,2-dichloro-ethane; for 48h; Reflux;
DOI:10.1021/ol9016222

Reference yield: 75.0%

: 5142-75-6
tri(p-tolyl)bismuth

: 100-20-9
terephthaloyl chloride

: 61565-13-7
1,4-phenylenebis[(4-methylphenyl)methanone]

Guidance literature:: With triethylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; at 80 ℃; for 3h;
DOI:10.1016/j.tet.2007.10.047