6-O-(6-O-acetyl-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1,3,4-tri-O-benzoyl-2-deoxy-2-phthalimido-α-D-glucopyranose

Base Information

Chemical Name:6-O-(6-O-acetyl-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1,3,4-tri-O-benzoyl-2-deoxy-2-phthalimido-α-D-glucopyranose
CAS No.:933791-00-5
Molecular Formula:C₆₅H₅₀N₂O₁₉
Molecular Weight:1163.11
Hs Code.:

Synonyms:6-O-(6-O-acetyl-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1,3,4-tri-O-benzoyl-2-deoxy-2-phthalimido-α-D-glucopyranose

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Chemical Property of 6-O-(6-O-acetyl-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1,3,4-tri-O-benzoyl-2-deoxy-2-phthalimido-α-D-glucopyranose

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Technology Process of 6-O-(6-O-acetyl-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1,3,4-tri-O-benzoyl-2-deoxy-2-phthalimido-α-D-glucopyranose

There total 7 articles about 6-O-(6-O-acetyl-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1,3,4-tri-O-benzoyl-2-deoxy-2-phthalimido-α-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 933790-95-5
1,3,4-tri-O-benzoyl-2-deoxy-2-phthalimido-α-D-glucopyranose

: 933790-97-7
C₃₀H₂₄NO₉Br

: 933791-00-5
6-O-(6-O-acetyl-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1,3,4-tri-O-benzoyl-2-deoxy-2-phthalimido-α-D-glucopyranose

Guidance literature:: With mercury(II) cyanide; mercury dibromide; In acetonitrile; at 20 ℃; for 1h;
DOI:10.1134/S1068162006040108

Reference yield:

: C₅₄H₄₃NO₁₁

: 933791-00-5
6-O-(6-O-acetyl-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1,3,4-tri-O-benzoyl-2-deoxy-2-phthalimido-α-D-glucopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine; acetic anhydride / 2 h / Heating

2: 4.7 g / aq. trifluoroacetic acid / CH₂Cl₂ / 1 h

3: 79 percent / mercury(II) cyanide; HgBr₂ / acetonitrile / 1 h / 20 °C

With pyridine; mercury(II) cyanide; acetic anhydride; trifluoroacetic acid; mercury dibromide; In dichloromethane; acetonitrile;
DOI:10.1134/S1068162006040108

Reference yield:

: C₅₄H₄₁NO₁₀

: 933791-00-5
6-O-(6-O-acetyl-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-1,3,4-tri-O-benzoyl-2-deoxy-2-phthalimido-α-D-glucopyranose

Guidance literature:: Multi-step reaction with 2 steps

1: 4.7 g / aq. trifluoroacetic acid / CH₂Cl₂ / 1 h

2: 79 percent / mercury(II) cyanide; HgBr₂ / acetonitrile / 1 h / 20 °C

With mercury(II) cyanide; trifluoroacetic acid; mercury dibromide; In dichloromethane; acetonitrile;
DOI:10.1134/S1068162006040108