3-(benzyloxycarbonylamino)propyl-6-O-(3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranose

Base Information

Chemical Name:3-(benzyloxycarbonylamino)propyl-6-O-(3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranose
CAS No.:933791-01-6
Molecular Formula:C₆₇H₅₇N₃O₁₉
Molecular Weight:1208.2
Hs Code.:

3-(benzyloxycarbonylamino)propyl-6-O-(3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranose

Synonyms:3-(benzyloxycarbonylamino)propyl-6-O-(3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranose

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Chemical Property of 3-(benzyloxycarbonylamino)propyl-6-O-(3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranose

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Technology Process of 3-(benzyloxycarbonylamino)propyl-6-O-(3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranose

There total 10 articles about 3-(benzyloxycarbonylamino)propyl-6-O-(3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₅₄H₄₃NO₁₁

: 933791-01-6
3-(benzyloxycarbonylamino)propyl-6-O-(3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine; acetic anhydride / 2 h / Heating

2: 4.7 g / aq. trifluoroacetic acid / CH₂Cl₂ / 1 h

3: 79 percent / mercury(II) cyanide; HgBr₂ / acetonitrile / 1 h / 20 °C

4: HBr; AcOH / CH₂Cl₂ / 16 h

5: mercury(II) cyanide; HgBr₂ / acetonitrile / 1 h / 20 °C

6: 80 mg / acetyl chloride; methanol / CH₂Cl₂ / 16 h / 20 °C

With pyridine; methanol; hydrogen bromide; mercury(II) cyanide; acetic anhydride; acetic acid; acetyl chloride; trifluoroacetic acid; mercury dibromide; In dichloromethane; acetonitrile;
DOI:10.1134/S1068162006040108

Reference yield:

: 933790-95-5
1,3,4-tri-O-benzoyl-2-deoxy-2-phthalimido-α-D-glucopyranose

: 933791-01-6
3-(benzyloxycarbonylamino)propyl-6-O-(3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: 79 percent / mercury(II) cyanide; HgBr₂ / acetonitrile / 1 h / 20 °C

2: HBr; AcOH / CH₂Cl₂ / 16 h

3: mercury(II) cyanide; HgBr₂ / acetonitrile / 1 h / 20 °C

4: 80 mg / acetyl chloride; methanol / CH₂Cl₂ / 16 h / 20 °C

With methanol; hydrogen bromide; mercury(II) cyanide; acetic acid; acetyl chloride; mercury dibromide; In dichloromethane; acetonitrile;
DOI:10.1134/S1068162006040108

Reference yield:

: C₅₄H₄₁NO₁₀

: 933791-01-6
3-(benzyloxycarbonylamino)propyl-6-O-(3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranosyl)-3,4-di-O-benzoyl-2-deoxy-2-phthalimido-β-D-glucopyranose

Guidance literature:: Multi-step reaction with 5 steps

1: 4.7 g / aq. trifluoroacetic acid / CH₂Cl₂ / 1 h

2: 79 percent / mercury(II) cyanide; HgBr₂ / acetonitrile / 1 h / 20 °C

3: HBr; AcOH / CH₂Cl₂ / 16 h

4: mercury(II) cyanide; HgBr₂ / acetonitrile / 1 h / 20 °C

5: 80 mg / acetyl chloride; methanol / CH₂Cl₂ / 16 h / 20 °C

With methanol; hydrogen bromide; mercury(II) cyanide; acetic acid; acetyl chloride; trifluoroacetic acid; mercury dibromide; In dichloromethane; acetonitrile;
DOI:10.1134/S1068162006040108