C₃₂H₂₂S₈

Base Information

Chemical Name:C₃₂H₂₂S₈
CAS No.:1280592-13-3
Molecular Formula:C₃₂H₂₂S₈
Molecular Weight:663.055
Hs Code.:

C<sub>32</sub>H<sub>22</sub>S<sub>8</sub>

Synonyms:C₃₂H₂₂S₈

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Chemical Property of C₃₂H₂₂S₈

Chemical Property:

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Technology Process of C₃₂H₂₂S₈

There total 4 articles about C₃₂H₂₂S₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1280592-10-0
C₁₉H₂₀S₄Si

: 1280592-13-3
C₃₂H₂₂S₈

Guidance literature:: C₁₉H₂₀S₄Si; With potassium carbonate; In tetrahydrofuran; methanol; at 20 ℃; for 0.5h;

With copper(l) iodide; N,N,N,N,-tetramethylethylenediamine; In dichloromethane; at 20 ℃; for 3h;
DOI:10.1021/jo2000447

Reference yield:

: 138519-02-5
dimethyl 4,5-bis(methylthio)-1,3-dithiole phosphonate ester

: 1280592-13-3
C₃₂H₂₂S₈

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran / 0.33 h / -78 °C

1.2: -78 - 20 °C

2.1: potassium carbonate / tetrahydrofuran; methanol / 0.5 h / 20 °C

2.2: 3 h / 20 °C

3.1: potassium carbonate / tetrahydrofuran; methanol / 0.5 h / 20 °C

3.2: 3 h / 20 °C

With n-butyllithium; potassium carbonate; In tetrahydrofuran; methanol; 1.2: Horner-Wadsworth-Emmons reaction / 2.2: Hay coupling / 3.2: Hay coupling;
DOI:10.1021/jo2000447

Reference yield:

: 1207513-37-8
C₁₇H₂₀S₄Si

: 1280592-13-3
C₃₂H₂₂S₈

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / tetrahydrofuran; methanol / 0.5 h / 20 °C

1.2: 3 h / 20 °C

2.1: potassium carbonate / tetrahydrofuran; methanol / 0.5 h / 20 °C

2.2: 3 h / 20 °C

With potassium carbonate; In tetrahydrofuran; methanol; 1.2: Hay coupling / 2.2: Hay coupling;
DOI:10.1021/jo2000447