(S)-methyl-3-methyl-2-(4-methyl-N-((S)-2-(2-(4-methyl-N-((S)-2-(4-methylphenylsulfonamido)-3-phenylpropyl)phenylsulfonamido)phenylamino)-3-phenylpropyl)phenylsulfonamido)butanoate

Base Information

Chemical Name:(S)-methyl-3-methyl-2-(4-methyl-N-((S)-2-(2-(4-methyl-N-((S)-2-(4-methylphenylsulfonamido)-3-phenylpropyl)phenylsulfonamido)phenylamino)-3-phenylpropyl)phenylsulfonamido)butanoate
CAS No.:1360632-26-3
Molecular Formula:C₅₁H₅₈N₄O₈S₃
Molecular Weight:951.242
Hs Code.:

(S)-methyl-3-methyl-2-(4-methyl-N-((S)-2-(2-(4-methyl-N-((S)-2-(4-methylphenylsulfonamido)-3-phenylpropyl)phenylsulfonamido)phenylamino)-3-phenylpropyl)phenylsulfonamido)butanoate

Synonyms:(S)-methyl-3-methyl-2-(4-methyl-N-((S)-2-(2-(4-methyl-N-((S)-2-(4-methylphenylsulfonamido)-3-phenylpropyl)phenylsulfonamido)phenylamino)-3-phenylpropyl)phenylsulfonamido)butanoate

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Chemical Property of (S)-methyl-3-methyl-2-(4-methyl-N-((S)-2-(2-(4-methyl-N-((S)-2-(4-methylphenylsulfonamido)-3-phenylpropyl)phenylsulfonamido)phenylamino)-3-phenylpropyl)phenylsulfonamido)butanoate

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Technology Process of (S)-methyl-3-methyl-2-(4-methyl-N-((S)-2-(2-(4-methyl-N-((S)-2-(4-methylphenylsulfonamido)-3-phenylpropyl)phenylsulfonamido)phenylamino)-3-phenylpropyl)phenylsulfonamido)butanoate

There total 10 articles about (S)-methyl-3-methyl-2-(4-methyl-N-((S)-2-(2-(4-methyl-N-((S)-2-(4-methylphenylsulfonamido)-3-phenylpropyl)phenylsulfonamido)phenylamino)-3-phenylpropyl)phenylsulfonamido)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 952060-26-3
N-(2-nitrophenyl)-phenylalanine

: 1360632-26-3
(S)-methyl-3-methyl-2-(4-methyl-N-((S)-2-(2-(4-methyl-N-((S)-2-(4-methylphenylsulfonamido)-3-phenylpropyl)phenylsulfonamido)phenylamino)-3-phenylpropyl)phenylsulfonamido)butanoate

Guidance literature:: Multi-step reaction with 8 steps

1: thionyl chloride / 0 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 0.08 h / 0 - 20 °C

3: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

4: palladium 10% on activated carbon; hydrogen / methanol / 1 h / 2585.81 Torr / Inert atmosphere

5: pyridine / 12 h / 0 °C

6: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

7: thionyl chloride / methanol / 0.08 h / 20 °C

8: pyridine / 12 h / 0 °C

With pyridine; lithium aluminium tetrahydride; thionyl chloride; palladium 10% on activated carbon; hydrogen; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; 3: Mitsunobu reaction / 6: Mitsunobu reaction;
DOI:10.1039/c1ob06304a

Reference yield:

: 1132769-58-4
(2S)-2-(2-nitrophenylamino)-3-phenylpropionic acid methyl ester

: 1360632-26-3
(S)-methyl-3-methyl-2-(4-methyl-N-((S)-2-(2-(4-methyl-N-((S)-2-(4-methylphenylsulfonamido)-3-phenylpropyl)phenylsulfonamido)phenylamino)-3-phenylpropyl)phenylsulfonamido)butanoate

Guidance literature:: Multi-step reaction with 7 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 0.08 h / 0 - 20 °C

2: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

3: palladium 10% on activated carbon; hydrogen / methanol / 1 h / 2585.81 Torr / Inert atmosphere

4: pyridine / 12 h / 0 °C

5: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

6: thionyl chloride / methanol / 0.08 h / 20 °C

7: pyridine / 12 h / 0 °C

With pyridine; lithium aluminium tetrahydride; thionyl chloride; palladium 10% on activated carbon; hydrogen; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; 2: Mitsunobu reaction / 5: Mitsunobu reaction;
DOI:10.1039/c1ob06304a

Reference yield:

: 1313392-74-3
(S)-2-(2-nitro-phenylamino)-3-phenyl-propan-1-ol

: 1360632-26-3
(S)-methyl-3-methyl-2-(4-methyl-N-((S)-2-(2-(4-methyl-N-((S)-2-(4-methylphenylsulfonamido)-3-phenylpropyl)phenylsulfonamido)phenylamino)-3-phenylpropyl)phenylsulfonamido)butanoate

Guidance literature:: Multi-step reaction with 6 steps

1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

2: palladium 10% on activated carbon; hydrogen / methanol / 1 h / 2585.81 Torr / Inert atmosphere

3: pyridine / 12 h / 0 °C

4: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

5: thionyl chloride / methanol / 0.08 h / 20 °C

6: pyridine / 12 h / 0 °C

With pyridine; thionyl chloride; palladium 10% on activated carbon; hydrogen; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; methanol; 1: Mitsunobu reaction / 4: Mitsunobu reaction;
DOI:10.1039/c1ob06304a