Technology Process of octyl 2,6-di-O-benzyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside
There total 6 articles about octyl 2,6-di-O-benzyl-β-D-galactopyranosyl-(1->4)-2,3,6-tri-O-benzyl-β-D-glucopyranoside which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 5 steps
1.1: AgClO4; 4 Angstroem molecular sieves; Ag2CO3 / 24 h / 20 °C
1.2: aq. TFA / CH2Cl2
2.1: 99 percent / Na / methanol / 1 h / 20 °C
3.1: p-TsOH / 60 h / 20 °C
3.2: 66 percent / aq. TFA / ethyl acetate / 1 h
4.1: 95 percent / NaH / dimethylformamide / 0 - 20 °C
5.1: 98 percent / aq. AcOH / 2 h / 80 °C
With
4 A molecular sieve; silver perchlorate; sodium; sodium hydride; toluene-4-sulfonic acid; acetic acid; silver carbonate;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(02)00265-X
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 44 percent / AgClO4; 4 Angstroem molecular sieves; Ag2CO3 / CH2Cl2 / 24 h / 20 °C
2.1: 99 percent / Na / methanol / 1 h / 20 °C
3.1: p-TsOH / 60 h / 20 °C
3.2: 66 percent / aq. TFA / ethyl acetate / 1 h
4.1: 95 percent / NaH / dimethylformamide / 0 - 20 °C
5.1: 98 percent / aq. AcOH / 2 h / 80 °C
With
4 A molecular sieve; silver perchlorate; sodium; sodium hydride; toluene-4-sulfonic acid; acetic acid; silver carbonate;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4020(02)00265-X
