5-acetoxyhexyl phenyl sulfide

Base Information

Chemical Name:5-acetoxyhexyl phenyl sulfide
CAS No.:77657-99-9
Molecular Formula:C₁₄H₂₀O₂S
Molecular Weight:252.378
Hs Code.:

Synonyms:5-acetoxyhexyl phenyl sulfide

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Chemical Property of 5-acetoxyhexyl phenyl sulfide

Chemical Property:

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Technology Process of 5-acetoxyhexyl phenyl sulfide

There total 1 articles about 5-acetoxyhexyl phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 930-69-8
sodium thiophenolate

: 344325-55-9
5-acetoxy-1-bromohexane

: 77657-99-9
5-acetoxyhexyl phenyl sulfide

Guidance literature:: DOI:10.1246/bcsj.53.3615

Reference yield: 95.0%

: 77657-99-9
5-acetoxyhexyl phenyl sulfide

: 77657-89-7
6-phenylthio-2-hexanol

Guidance literature:: With potassium hydroxide; In 1,4-dioxane; for 5h; Heating;
DOI:10.1246/bcsj.53.3615

Reference yield:

: 77657-99-9
5-acetoxyhexyl phenyl sulfide

: 101704-30-7,101704-35-2,125334-92-1,125334-93-2
(1SR,2RS)-1-methyl-2-phenylthiocyclopentanol

: 101704-30-7,101704-35-2,125334-92-1,125334-93-2
(1RS,2RS)-1-methyl-2-phenylthiocyclopentanol

Guidance literature:: With N-chloro-succinimide; methyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1.) CCl₄, 2.) THF, -80 deg C, allowed to warm to RT;
DOI:10.1016/S0040-4039(00)88936-4