[[Ph₂B(CH₂PPh₂)2]Pt(Me)2][ASN]

Base Information

Chemical Name:[[Ph₂B(CH₂PPh₂)2]Pt(Me)2][ASN]
CAS No.:350480-02-3
Molecular Formula:C₈H₁₆N*C₄₀H₄₀BP₂Pt
Molecular Weight:914.818
Hs Code.:

[[Ph<sub>2</sub>B(CH<sub>2</sub>PPh<sub>2</sub>)2]Pt(Me)2][ASN]

Synonyms:[[Ph₂B(CH₂PPh₂)2]Pt(Me)2][ASN]

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Chemical Property of [[Ph₂B(CH₂PPh₂)2]Pt(Me)2][ASN]

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Technology Process of [[Ph₂B(CH₂PPh₂)2]Pt(Me)2][ASN]

There total 1 articles about [[Ph₂B(CH₂PPh₂)2]Pt(Me)2][ASN] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.4%

: (1,5-cyclooctadiene)dimethylplatinum(II)

: 350480-00-1
5-azonia-spiro[4.4]nonane bis(diphenylphosphinomethyl)diphenylborate

: 350480-02-3
[[Ph₂B(CH₂PPh₂)2]Pt(Me)2][ASN]

Guidance literature:: In tetrahydrofuran; under inert atm. (COD)PtMe2 and (Ph2B(CH2PPh2)2)(ASN) were mixed in THF and stirred for 1 h; react. mixt. was concd. under reduced pressure and triturated with pentane, residue was dried in vacuo; elem. anal.;
DOI:10.1021/ja0296071

Reference yield: 86.3%

: 350480-02-3
[[Ph₂B(CH₂PPh₂)2]Pt(Me)2][ASN]

: 201230-82-2
carbon monoxide

: 577785-24-1
[(phenyl)2B(CH₂P(phenyl)2)2]Pt(methyl)(carbon monoxide)

Guidance literature:: With [Et₃NH][BPh₄]; In tetrahydrofuran; under inert atm. THF soln. (Et3NH)(BPh4) was added to stirred THF soln. ((Ph2B(CH2PPh2)2)(ASN) and stirred for 15 min, ppt. was filtered off, stream CO was passed through filtrate; volatiles were removed in vacuo, residue was dissolved in THF, filtered,concd., triturated with pentane, washed with Et2O, and dried under redu ced pressure; elem. anal.;
DOI:10.1021/ja0296071

Reference yield:

: 350480-02-3
[[Ph₂B(CH₂PPh₂)2]Pt(Me)2][ASN]

: [B(C₆H₅)2(PCH₂(C₆H₅)2)2Pt(CH₃)(C₅H₅N)]

Guidance literature:: Multi-step reaction with 2 steps

1: [((CH₃)2CH)2(C₂H₅)NH][B(C₆H₅)4] / tetrahydrofuran

2: water

With [((CH₃)2CH)2(C₂H₅)NH][B(C₆H₅)4]; In tetrahydrofuran; water;
DOI:10.1021/ja0058987