C₂₉H₄₄O₅Si

Base Information

Chemical Name:C₂₉H₄₄O₅Si
CAS No.:1236311-60-6
Molecular Formula:C₂₉H₄₄O₅Si
Molecular Weight:500.751
Hs Code.:

C<sub>29</sub>H<sub>44</sub>O<sub>5</sub>Si

Synonyms:C₂₉H₄₄O₅Si

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Chemical Property of C₂₉H₄₄O₅Si

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Technology Process of C₂₉H₄₄O₅Si

There total 10 articles about C₂₉H₄₄O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 67373-56-2
chlorodimethyl(1,1,2-trimethylpropyl)silane

: 207564-35-0
3,4-di-O-benzyl-5a-carba-α-D-glucopyranose

: 1236311-60-6
C₂₉H₄₄O₅Si

Guidance literature:: With 1H-imidazole; In tetrahydrofuran; at 15 - 20 ℃; for 24h; regioselective reaction;
DOI:10.1039/c2ob25222h

Reference yield:

: C₁₄H₂₈O₄Si

: 1236311-60-6
C₂₉H₄₄O₅Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran / 2 h / 20 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 20 °C

3.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 4 h / 75 °C / Inert atmosphere

4.1: potassium hexamethylsilazane / tetrahydrofuran / 1.5 h / -78 - 0 °C / Inert atmosphere

4.2: 3 h / -78 - 20 °C / Inert atmosphere

5.1: 1,2-dichloro-benzene / 2 h / 240 °C / Sealed tube

6.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 0.25 h

7.1: osmium(VIII) oxide; trimethylamine-N-oxide / water; acetone / 48 h / 20 °C

8.1: 1H-imidazole / tetrahydrofuran / 24 h / 15 - 20 °C

With 1H-imidazole; sodium tetrahydroborate; osmium(VIII) oxide; trimethylamine-N-oxide; tetrabutyl ammonium fluoride; tetra-(n-butyl)ammonium iodide; potassium hexamethylsilazane; sodium hydride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; ethanol; water; ethyl acetate; 1,2-dichloro-benzene; acetone; 4.2: Wittig reaction;
DOI:10.1039/c2ob25222h

Reference yield:

: C₂₈H₄₀O₄Si

: 1236311-60-6
C₂₉H₄₄O₅Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 - 20 °C

2.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / ethyl acetate / 4 h / 75 °C / Inert atmosphere

3.1: potassium hexamethylsilazane / tetrahydrofuran / 1.5 h / -78 - 0 °C / Inert atmosphere

3.2: 3 h / -78 - 20 °C / Inert atmosphere

4.1: 1,2-dichloro-benzene / 2 h / 240 °C / Sealed tube

5.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / 0.25 h

6.1: osmium(VIII) oxide; trimethylamine-N-oxide / water; acetone / 48 h / 20 °C

7.1: 1H-imidazole / tetrahydrofuran / 24 h / 15 - 20 °C

With 1H-imidazole; sodium tetrahydroborate; osmium(VIII) oxide; trimethylamine-N-oxide; tetrabutyl ammonium fluoride; potassium hexamethylsilazane; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; ethanol; water; ethyl acetate; 1,2-dichloro-benzene; acetone; 3.2: Wittig reaction;
DOI:10.1039/c2ob25222h