(1S,3aR,7aR)-2-Oxo-2,3,3a,4,7,7a-hexahydro-1H-indene-1-carbothioic acid S-phenyl ester

Base Information

Chemical Name:(1S,3aR,7aR)-2-Oxo-2,3,3a,4,7,7a-hexahydro-1H-indene-1-carbothioic acid S-phenyl ester
CAS No.:113435-68-0
Molecular Formula:C₁₆H₁₆O₂S
Molecular Weight:272.368
Hs Code.:

Synonyms:(1S,3aR,7aR)-2-Oxo-2,3,3a,4,7,7a-hexahydro-1H-indene-1-carbothioic acid S-phenyl ester

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Chemical Property of (1S,3aR,7aR)-2-Oxo-2,3,3a,4,7,7a-hexahydro-1H-indene-1-carbothioic acid S-phenyl ester

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Technology Process of (1S,3aR,7aR)-2-Oxo-2,3,3a,4,7,7a-hexahydro-1H-indene-1-carbothioic acid S-phenyl ester

There total 4 articles about (1S,3aR,7aR)-2-Oxo-2,3,3a,4,7,7a-hexahydro-1H-indene-1-carbothioic acid S-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 112168-16-8
((1R,6S)-6-Phenylsulfanylcarbonylmethyl-cyclohex-3-enyl)-acetic acid methyl ester

: 113435-68-0
(1S,3aR,7aR)-2-Oxo-2,3,3a,4,7,7a-hexahydro-1H-indene-1-carbothioic acid S-phenyl ester

Guidance literature:: With aluminium trichloride; triethylamine; In dichloromethane; at 0 ℃;
DOI:10.1039/cc9960001775

Reference yield: 54.0%

: 112318-56-6
4(R)-methoxycarbonyl-1,3-thiazolidine-2-thione monoamide

: 113435-68-0
(1S,3aR,7aR)-2-Oxo-2,3,3a,4,7,7a-hexahydro-1H-indene-1-carbothioic acid S-phenyl ester

Guidance literature:: With potassium hydride; In tetrahydrofuran; for 10h; Ambient temperature;
DOI:10.1246/cl.1987.1861

Reference yield:

: 108-98-5
thiophenol

: 113435-68-0
(1S,3aR,7aR)-2-Oxo-2,3,3a,4,7,7a-hexahydro-1H-indene-1-carbothioic acid S-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / N,N'-carbonyldiimidazole / tetrahydrofuran

2: 61 percent / AlCl₃, Et₃N / CH₂Cl₂ / 0 °C

With aluminium trichloride; triethylamine; 1,1'-carbonyldiimidazole; In tetrahydrofuran; dichloromethane;
DOI:10.1039/cc9960001775