C₃₂H₄₈O₇Si

Base Information

Chemical Name:C₃₂H₄₈O₇Si
CAS No.:1352481-46-9
Molecular Formula:C₃₂H₄₈O₇Si
Molecular Weight:572.814
Hs Code.:

C<sub>32</sub>H<sub>48</sub>O<sub>7</sub>Si

Synonyms:C₃₂H₄₈O₇Si

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Chemical Property of C₃₂H₄₈O₇Si

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Technology Process of C₃₂H₄₈O₇Si

There total 19 articles about C₃₂H₄₈O₇Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1352481-44-7
C₃₂H₄₆O₇Si

: 1352481-46-9
C₃₂H₄₈O₇Si

Guidance literature:: With palladium on activated charcoal; hydrogen; In ethanol; at 20 ℃; Inert atmosphere;
DOI:10.1021/ol202966m

Reference yield:

: 1352481-47-0
C₃₂H₄₆O₇Si

: 1352481-46-9
C₃₂H₄₈O₇Si

Guidance literature:: With dimethylsulfide borane complex; (3aR)-1-methyl-3,3-diphenyl-tetrahydro-pyrrolo[1,2-c][1,3,2]oxazaborole; In tetrahydrofuran; at 20 ℃; for 0.333333h; Inert atmosphere;
DOI:10.1021/ol202966m

Reference yield:

: 27230-58-6
(5-bromo-2-furan-2-yl)methanol

: 1352481-46-9
C₃₂H₄₈O₇Si

Guidance literature:: Multi-step reaction with 10 steps

1.1: 1H-imidazole; dmap / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

2.1: lithium dicyclohexylamide / toluene / 0.17 h / 0 °C / Inert atmosphere

2.2: 20 °C / Inert atmosphere

3.1: diisobutylaluminium hydride / diethyl ether / 1 h / -78 °C / Inert atmosphere

4.1: di-n-butylboryl trifluoromethanesulfonate; N-ethyl-N,N-diisopropylamine / diethyl ether / 0.55 h / -100 °C / Inert atmosphere

4.2: 7 h / -100 - -78 °C / Inert atmosphere

5.1: tetramethylammonium triacetoxyborohydride / acetic acid; acetonitrile / 20 h / -20 °C / Inert atmosphere

6.1: dmap; triethylamine / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

7.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane; water / 1 h / Reflux; Inert atmosphere

8.1: dmap; triethylamine / dichloromethane / 4 h / 0 °C / Inert atmosphere

9.1: (1,1';3',1''-terphenyl)-2'-ol; trimethylaluminum / hexane; toluene / 0.33 h / -78 °C / Inert atmosphere

9.2: 0.5 h / -78 °C / Inert atmosphere

10.1: palladium on activated charcoal; hydrogen / ethanol / 20 °C / Inert atmosphere

With 1H-imidazole; dmap; di-n-butylboryl trifluoromethanesulfonate; (1,1';3',1''-terphenyl)-2'-ol; palladium on activated charcoal; hydrogen; trimethylaluminum; diisobutylaluminium hydride; lithium dicyclohexylamide; triethylamine; N-ethyl-N,N-diisopropylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; tetramethylammonium triacetoxyborohydride; In diethyl ether; ethanol; hexane; dichloromethane; water; acetic acid; N,N-dimethyl-formamide; toluene; acetonitrile; 4.1: Aldol reaction / 4.2: Aldol reaction;
DOI:10.1021/ol202966m