4-[(3,5,6-TRIMETHYL-2-PYRAZINYL)METHOXY]BENZOIC ACID ETHYL ESTER

Base Information

Chemical Name:4-[(3,5,6-TRIMETHYL-2-PYRAZINYL)METHOXY]BENZOIC ACID ETHYL ESTER
CAS No.:947243-80-3
Molecular Formula:C₁₇H₂₀N₂O₃
Molecular Weight:300.357
Hs Code.:
Mol file:947243-80-3.mol

Synonyms:ethyl 4-[(3,5,6-trimethylpyrazin-2-yl)methoxy]benzoate

Suppliers and Price of 4-[(3,5,6-TRIMETHYL-2-PYRAZINYL)METHOXY]BENZOIC ACID ETHYL ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-[(3,5,6-TRIMETHYL-2-PYRAZINYL)METHOXY]BENZOIC ACID ETHYL ESTER

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

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Technology Process of 4-[(3,5,6-TRIMETHYL-2-PYRAZINYL)METHOXY]BENZOIC ACID ETHYL ESTER

There total 3 articles about 4-[(3,5,6-TRIMETHYL-2-PYRAZINYL)METHOXY]BENZOIC ACID ETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.3%

: 120-47-8
Ethyl 4-hydroxybenzoate

: 79074-45-6
2-(bromomethyl)-3,5,6-trimethylpyrazine

: 947243-80-3
ethyl 4-[(3,5,6-trimethylpyrazin-2-yl)methoxy]benzoate

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 85 ℃; for 12h;

Reference yield:

: 76494-51-4
Tetramethylpyrazine hydrochloride

: 947243-80-3
ethyl 4-[(3,5,6-trimethylpyrazin-2-yl)methoxy]benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / water

2: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 10 h / 65 °C / Irradiation

3: N-benzyl-N,N,N-triethylammonium chloride; sodium carbonate / acetone / 24 h / Reflux

With N-Bromosuccinimide; N-benzyl-N,N,N-triethylammonium chloride; sodium carbonate; sodium hydroxide; dibenzoyl peroxide; In tetrachloromethane; water; acetone;
DOI:10.1002/cbdv.200900353

Reference yield:

: 1124-11-4
Tetramethylpyrazine

: 947243-80-3
ethyl 4-[(3,5,6-trimethylpyrazin-2-yl)methoxy]benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 10 h / 65 °C / Irradiation

2: N-benzyl-N,N,N-triethylammonium chloride; sodium carbonate / acetone / 24 h / Reflux

With N-Bromosuccinimide; N-benzyl-N,N,N-triethylammonium chloride; sodium carbonate; dibenzoyl peroxide; In tetrachloromethane; acetone;
DOI:10.1002/cbdv.200900353