Technology Process of 4-[(3,5,6-TRIMETHYL-2-PYRAZINYL)METHOXY]BENZOIC ACID ETHYL ESTER
There total 3 articles about 4-[(3,5,6-TRIMETHYL-2-PYRAZINYL)METHOXY]BENZOIC ACID ETHYL ESTER which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
N,N-dimethyl-formamide;
at 85 ℃;
for 12h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydroxide / water
2: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 10 h / 65 °C / Irradiation
3: N-benzyl-N,N,N-triethylammonium chloride; sodium carbonate / acetone / 24 h / Reflux
With
N-Bromosuccinimide; N-benzyl-N,N,N-triethylammonium chloride; sodium carbonate; sodium hydroxide; dibenzoyl peroxide;
In
tetrachloromethane; water; acetone;
DOI:10.1002/cbdv.200900353
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 10 h / 65 °C / Irradiation
2: N-benzyl-N,N,N-triethylammonium chloride; sodium carbonate / acetone / 24 h / Reflux
With
N-Bromosuccinimide; N-benzyl-N,N,N-triethylammonium chloride; sodium carbonate; dibenzoyl peroxide;
In
tetrachloromethane; acetone;
DOI:10.1002/cbdv.200900353