Technology Process of C27H46O5
There total 5 articles about C27H46O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C
2: lithium aluminium tetrahydride / diethyl ether / 1 h / 20 °C
With
lithium aluminium tetrahydride; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid;
In
diethyl ether; dichloromethane;
DOI:10.1016/j.steroids.2013.12.002
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 12 h / 20 °C
2.1: sodium tetrahydroborate; boron trifluoride diethyl etherate / tetrahydrofuran; diethylene glycol dimethyl ether / 6 h / 0 °C / Inert atmosphere
3.1: sodium hydrogencarbonate / water / 60 °C
3.2: 19 h / 20 - 85 °C
4.1: toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 20 °C
5.1: lithium aluminium tetrahydride / diethyl ether / 1 h / 20 °C
With
dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; sodium hydrogencarbonate; toluene-4-sulfonic acid; 3-chloro-benzenecarboperoxoic acid; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; diethyl ether; dichloromethane; diethylene glycol dimethyl ether; water;
DOI:10.1016/j.steroids.2013.12.002
