1-[3-[[(diphenylphosphinyl)acetyl]amino]propyl]-3-tetradecyl-1H-imidazol-3-ium bromide

Base Information

• Chemical Name: 1-[3-[[(diphenylphosphinyl)acetyl]amino]propyl]-3-tetradecyl-1H-imidazol-3-ium bromide
• CAS No.: 1228996-18-6
• Molecular Formula: Br*C₃₄H₅₁N₃O₂P
• Molecular Weight: 644.676
• Mol file: 1228996-18-6.mol

Synonyms:1-[3-[[(diphenylphosphinyl)acetyl]amino]propyl]-3-tetradecyl-1H-imidazol-3-ium bromide

Chemical Property of 1-[3-[[(diphenylphosphinyl)acetyl]amino]propyl]-3-tetradecyl-1H-imidazol-3-ium bromide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-[3-[[(diphenylphosphinyl)acetyl]amino]propyl]-3-tetradecyl-1H-imidazol-3-ium bromide

There total 3 articles about 1-[3-[[(diphenylphosphinyl)acetyl]amino]propyl]-3-tetradecyl-1H-imidazol-3-ium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

1-Bromotetradecane (112-71-0) + 2-(diphenylphosphinyl)-N-[3-(1H-imidazol-1-yl)propyl]-acetamide (1228996-38-0) → 1-[3-[[(diphenylphosphinyl)acetyl]amino]propyl]-3-tetradecyl-1H-imidazol-3-ium bromide (1228996-18-6)

Guidance literature:

In acetonitrile; at 0 - 85 ℃; Inert atmosphere;

DOI:10.1039/b926377b

Reference yield:

ethyl 2-(diphenylphosphoryl)acetate (6361-05-3) → 1-[3-[[(diphenylphosphinyl)acetyl]amino]propyl]-3-tetradecyl-1H-imidazol-3-ium bromide (1228996-18-6)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol; water / 72 h / Reflux; Sealed tube

2: acetonitrile / 0 - 85 °C / Inert atmosphere

In ethanol; water; acetonitrile;

DOI:10.1039/b926377b

Reference yield:

3-(1H-imidazol-1-yl)propan-1-amine (5036-48-6) → 1-[3-[[(diphenylphosphinyl)acetyl]amino]propyl]-3-tetradecyl-1H-imidazol-3-ium bromide (1228996-18-6)

Guidance literature:

Multi-step reaction with 2 steps

1: ethanol; water / 72 h / Reflux; Sealed tube

2: acetonitrile / 0 - 85 °C / Inert atmosphere

In ethanol; water; acetonitrile;

DOI:10.1039/b926377b

upstream raw materials:

3-(1H-imidazol-1-yl)propan-1-amine

1-Bromotetradecane

2-(diphenylphosphinyl)-N-[3-(1H-imidazol-1-yl)propyl]-acetamide

ethyl 2-(diphenylphosphoryl)acetate