(11S,12R)-11,12-Diphenyl-1,4,7-trioxa-10,13-diaza-cyclopentadecane

Base Information

• Chemical Name: (11S,12R)-11,12-Diphenyl-1,4,7-trioxa-10,13-diaza-cyclopentadecane
• CAS No.: 143062-15-1
• Molecular Formula: C₂₂H₃₀N₂O₃
• Molecular Weight: 370.492
• Mol file: 143062-15-1.mol

Synonyms:(11S,12R)-11,12-Diphenyl-1,4,7-trioxa-10,13-diaza-cyclopentadecane

Chemical Property of (11S,12R)-11,12-Diphenyl-1,4,7-trioxa-10,13-diaza-cyclopentadecane

Chemical Property:

Purity/Quality:

Safty Information:

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• Hazard Codes: 

MSDS Files:

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Technology Process of (11S,12R)-11,12-Diphenyl-1,4,7-trioxa-10,13-diaza-cyclopentadecane

There total 10 articles about (11S,12R)-11,12-Diphenyl-1,4,7-trioxa-10,13-diaza-cyclopentadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[1-Phenyl-meth-(E)-ylidene]-(2-{2-[2-(2-{[1-phenyl-meth-(E)-ylidene]-amino}-ethoxy)-ethoxy]-ethoxy}-ethyl)-amine → (11S,12R)-11,12-Diphenyl-1,4,7-trioxa-10,13-diaza-cyclopentadecane (143062-15-1) + (11R,12R)-11,12-Diphenyl-1,4,7-trioxa-10,13-diaza-cyclopentadecane (143029-10-1,143062-15-1)

Guidance literature:

With methanesulfonic acid; In N,N-dimethyl-formamide; at 25 ℃; Yield given. Yields of byproduct given; electroreduction;

DOI:10.1021/jo00118a013

Reference yield:

[1-Phenyl-meth-(E)-ylidene]-(2-{2-[2-(2-{[1-phenyl-meth-(E)-ylidene]-amino}-ethoxy)-ethoxy]-ethoxy}-ethyl)-amine → (11S,12R)-11,12-Diphenyl-1,4,7-trioxa-10,13-diaza-cyclopentadecane (143062-15-1) + (11R,12R)-11,12-Diphenyl-1,4,7-trioxa-10,13-diaza-cyclopentadecane (143029-10-1,143062-15-1)

Guidance literature:

With methanesulfonic acid; In N,N-dimethyl-formamide; at 25 ℃; Yield given. Yields of byproduct given; electroreduction;

DOI:10.1021/jo00118a013

Reference yield:

[1-Phenyl-meth-(E)-ylidene]-(2-{2-[2-(2-{[1-phenyl-meth-(E)-ylidene]-amino}-ethoxy)-ethoxy]-ethoxy}-ethyl)-amine (143029-06-5) → (11S,12R)-11,12-Diphenyl-1,4,7-trioxa-10,13-diaza-cyclopentadecane (143062-15-1) + (11R,12R)-11,12-Diphenyl-1,4,7-trioxa-10,13-diaza-cyclopentadecane (143029-10-1,143062-15-1)

Guidance literature:

With methanesulfonic acid; tetraethylammonium tosylate; In N,N-dimethyl-formamide; at 25 ℃; Yield given. Yields of byproduct given; electroreduction;

DOI:10.1016/S0040-4039(00)92085-9

upstream raw materials:

1,11-dichloro-3,6,9-trioxaundecane

1,2-Diphenylethylenediamine

[1-Phenyl-meth-(E)-ylidene]-(2-{2-[2-(2-{[1-phenyl-meth-(E)-ylidene]-amino}-ethoxy)-ethoxy]-ethoxy}-ethyl)-amine

2-[2-[2-[2-aminoethoxy]ethoxy]ethoxy]ethylamine