quinone-trimethyllock-C₂-diamine-Boc

Base Information

Chemical Name:quinone-trimethyllock-C₂-diamine-Boc
CAS No.:1111328-02-9
Molecular Formula:C₂₃H₃₆N₂O₅
Molecular Weight:420.549
Hs Code.:

quinone-trimethyllock-C<sub>2</sub>-diamine-Boc

Synonyms:quinone-trimethyllock-C₂-diamine-Boc

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Chemical Property of quinone-trimethyllock-C₂-diamine-Boc

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Technology Process of quinone-trimethyllock-C₂-diamine-Boc

There total 8 articles about quinone-trimethyllock-C₂-diamine-Boc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 40662-29-1
3-methyl-3-(2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienyl)-butyric acid

: 112257-19-9
tert-butyl N-methyl-N-<2-(methylamino)ethyl>carbamate

: 1111328-02-9
quinone-trimethyllock-C₂-diamine-Boc

Guidance literature:: 3-methyl-3-(2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienyl)-butyric acid; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at 0 ℃; for 0.5h;

tert-butyl N-methyl-N-<2-(methylamino)ethyl>carbamate; In tetrahydrofuran; at 20 ℃; for 24h;
DOI:10.1016/j.bioorg.2020.104200

Reference yield: 75.0%

: 40662-29-1
3-methyl-3-(2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienyl)-butyric acid

: N-methyl-N-(2-(methylamino)ethyl)carbamate tert-butyl ester hydrochloride

: 1111328-02-9
quinone-trimethyllock-C₂-diamine-Boc

Guidance literature:: 3-methyl-3-(2,4,5-trimethyl-3,6-dioxo-cyclohexa-1,4-dienyl)-butyric acid; With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at 0 ℃; for 0.5h;

N-methyl-N-(2-(methylamino)ethyl)carbamate tert-butyl ester hydrochloride; In tetrahydrofuran;

Reference yield:

: 700-13-0
Trimethylhydroquinone

: 1111328-02-9
quinone-trimethyllock-C₂-diamine-Boc

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene-4-sulfonic acid / 1.5 h / 70 °C

1.2: 1 h / 20 °C

2.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 16 h / 20 °C

With dmap; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; In dichloromethane;
DOI:10.1039/c8cc01715h