(Z)-1-(4-(benzyloxy)-2-bromo-5-methoxystyryl)-2-bromo-3-isopropoxy-4-methoxybenzene

Base Information

Chemical Name:(Z)-1-(4-(benzyloxy)-2-bromo-5-methoxystyryl)-2-bromo-3-isopropoxy-4-methoxybenzene
CAS No.:1417801-80-9
Molecular Formula:C₂₆H₂₆Br₂O₄
Molecular Weight:562.298
Hs Code.:

Synonyms:(Z)-1-(4-(benzyloxy)-2-bromo-5-methoxystyryl)-2-bromo-3-isopropoxy-4-methoxybenzene

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Chemical Property of (Z)-1-(4-(benzyloxy)-2-bromo-5-methoxystyryl)-2-bromo-3-isopropoxy-4-methoxybenzene

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Technology Process of (Z)-1-(4-(benzyloxy)-2-bromo-5-methoxystyryl)-2-bromo-3-isopropoxy-4-methoxybenzene

There total 3 articles about (Z)-1-(4-(benzyloxy)-2-bromo-5-methoxystyryl)-2-bromo-3-isopropoxy-4-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1417801-83-2
(4-(benzyloxy)-2-bromo-5-methoxybenzyl)triphenylphosphonium bromide

: 93710-50-0
2-bromo-3-isopropoxy-4-methoxybenzaldehyde

: 1417801-80-9
(Z)-1-(4-(benzyloxy)-2-bromo-5-methoxystyryl)-2-bromo-3-isopropoxy-4-methoxybenzene

Guidance literature:: (4-(benzyloxy)-2-bromo-5-methoxybenzyl)triphenylphosphonium bromide; With potassium tert-butylate; In tetrahydrofuran; at 0 - 20 ℃; for 1.5h; Inert atmosphere;

2-bromo-3-isopropoxy-4-methoxybenzaldehyde; In tetrahydrofuran; at 0 ℃; for 5h; Inert atmosphere;
DOI:10.1021/ol303390a

Reference yield:

: 222622-96-0
5-(benzyloxy)-1-bromo-2-(bromomethyl)-4-methoxybenzene

: 1417801-80-9
(Z)-1-(4-(benzyloxy)-2-bromo-5-methoxystyryl)-2-bromo-3-isopropoxy-4-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzene / 12 h / 80 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere

2.2: 5 h / 0 °C / Inert atmosphere

With potassium tert-butylate; In tetrahydrofuran; benzene;
DOI:10.1021/ol303390a

Reference yield:

: 2973-58-2
2-bromoisovanillin

: 1417801-80-9
(Z)-1-(4-(benzyloxy)-2-bromo-5-methoxystyryl)-2-bromo-3-isopropoxy-4-methoxybenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetra-(n-butyl)ammonium iodide; potassium carbonate / N,N-dimethyl-formamide / 3 h / 50 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere

2.2: 5 h / 0 °C / Inert atmosphere

With potassium tert-butylate; tetra-(n-butyl)ammonium iodide; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ol303390a