1-(4-(benzyloxy)-2-bromo-5-methoxyphenethyl)-2-bromo-3-isopropoxy-4-methoxybenzene

Base Information

Chemical Name:1-(4-(benzyloxy)-2-bromo-5-methoxyphenethyl)-2-bromo-3-isopropoxy-4-methoxybenzene
CAS No.:1417801-81-0
Molecular Formula:C₂₆H₂₈Br₂O₄
Molecular Weight:564.314
Hs Code.:

Synonyms:1-(4-(benzyloxy)-2-bromo-5-methoxyphenethyl)-2-bromo-3-isopropoxy-4-methoxybenzene

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Chemical Property of 1-(4-(benzyloxy)-2-bromo-5-methoxyphenethyl)-2-bromo-3-isopropoxy-4-methoxybenzene

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Technology Process of 1-(4-(benzyloxy)-2-bromo-5-methoxyphenethyl)-2-bromo-3-isopropoxy-4-methoxybenzene

There total 4 articles about 1-(4-(benzyloxy)-2-bromo-5-methoxyphenethyl)-2-bromo-3-isopropoxy-4-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1417801-80-9
(Z)-1-(4-(benzyloxy)-2-bromo-5-methoxystyryl)-2-bromo-3-isopropoxy-4-methoxybenzene

: 1417801-81-0
1-(4-(benzyloxy)-2-bromo-5-methoxyphenethyl)-2-bromo-3-isopropoxy-4-methoxybenzene

Guidance literature:: With water; sodium acetate; benzenesufonyl hydrazide; In tetrahydrofuran; for 24h; Inert atmosphere;
DOI:10.1021/ol303390a

Reference yield:

: 222622-96-0
5-(benzyloxy)-1-bromo-2-(bromomethyl)-4-methoxybenzene

: 1417801-81-0
1-(4-(benzyloxy)-2-bromo-5-methoxyphenethyl)-2-bromo-3-isopropoxy-4-methoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzene / 12 h / 80 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere

2.2: 5 h / 0 °C / Inert atmosphere

3.1: benzenesufonyl hydrazide; sodium acetate; water / tetrahydrofuran / 24 h / Inert atmosphere

With potassium tert-butylate; water; sodium acetate; benzenesufonyl hydrazide; In tetrahydrofuran; benzene;
DOI:10.1021/ol303390a

Reference yield:

: 2973-58-2
2-bromoisovanillin

: 1417801-81-0
1-(4-(benzyloxy)-2-bromo-5-methoxyphenethyl)-2-bromo-3-isopropoxy-4-methoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetra-(n-butyl)ammonium iodide; potassium carbonate / N,N-dimethyl-formamide / 3 h / 50 °C / Inert atmosphere

2.1: potassium tert-butylate / tetrahydrofuran / 1.5 h / 0 - 20 °C / Inert atmosphere

2.2: 5 h / 0 °C / Inert atmosphere

3.1: benzenesufonyl hydrazide; sodium acetate; water / tetrahydrofuran / 24 h / Inert atmosphere

With potassium tert-butylate; water; sodium acetate; tetra-(n-butyl)ammonium iodide; potassium carbonate; benzenesufonyl hydrazide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ol303390a