N,N-bis(3,4-dimethoxycarbonylcaffeoyl)-D,L-2,3-diaminopropionic acid methyl ester

Base Information

Chemical Name:N,N-bis(3,4-dimethoxycarbonylcaffeoyl)-D,L-2,3-diaminopropionic acid methyl ester
CAS No.:897932-01-3
Molecular Formula:C₃₀H₃₀N₂O₁₆
Molecular Weight:674.572
Hs Code.:

Synonyms:N,N-bis(3,4-dimethoxycarbonylcaffeoyl)-D,L-2,3-diaminopropionic acid methyl ester

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Chemical Property of N,N-bis(3,4-dimethoxycarbonylcaffeoyl)-D,L-2,3-diaminopropionic acid methyl ester

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Technology Process of N,N-bis(3,4-dimethoxycarbonylcaffeoyl)-D,L-2,3-diaminopropionic acid methyl ester

There total 2 articles about N,N-bis(3,4-dimethoxycarbonylcaffeoyl)-D,L-2,3-diaminopropionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.0%

: 16180-95-3
3,4-O-dimethoxycarbonyl caffeic acid chloride

: 6059-44-5,106973-48-2,147857-43-0
methyl 2,3-diaminopropanoate dihydrochloride

: 897932-01-3
N,N-bis(3,4-dimethoxycarbonylcaffeoyl)-D,L-2,3-diaminopropionic acid methyl ester

Guidance literature:: With pyridine; In benzene; for 0.5h;
DOI:10.1021/jm010359d

Reference yield:

: 18959-40-5
3,4-O-dimethoxycarbonyl caffeic acid

: 897932-01-3
N,N-bis(3,4-dimethoxycarbonylcaffeoyl)-D,L-2,3-diaminopropionic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂ / 80 - 90 °C

2: 14 percent / pyridine / benzene / 0.5 h

With pyridine; thionyl chloride; In benzene;
DOI:10.1021/jm010359d