ethyl 2-anilinomethylideneamino-6-isopropyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxylate

Base Information

Chemical Name:ethyl 2-anilinomethylideneamino-6-isopropyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxylate
CAS No.:1415734-55-2
Molecular Formula:C₂₀H₂₅N₃O₂S
Molecular Weight:371.503
Hs Code.:

Synonyms:ethyl 2-anilinomethylideneamino-6-isopropyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxylate

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Chemical Property of ethyl 2-anilinomethylideneamino-6-isopropyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxylate

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Technology Process of ethyl 2-anilinomethylideneamino-6-isopropyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxylate

There total 1 articles about ethyl 2-anilinomethylideneamino-6-isopropyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 74022-33-6
2-Amino-3-ethoxycarbonyl-4,5,6,7-tetrahydro-6-isopropylthieno<3,4-b>pyridine

: 122-51-0
orthoformic acid triethyl ester

: 62-53-3
aniline

: 1415734-55-2
ethyl 2-anilinomethylideneamino-6-isopropyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxylate

Guidance literature:: 2-Amino-3-ethoxycarbonyl-4,5,6,7-tetrahydro-6-isopropylthieno<3,4-b>pyridine; orthoformic acid triethyl ester; In toluene; Reflux;

aniline; In toluene; Reflux;
DOI:10.1007/s11172-012-0052-3

Reference yield: 37.0%

: 1415734-55-2
ethyl 2-anilinomethylideneamino-6-isopropyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxylate

: 1415734-49-4
7-isopropyl-3-phenyl-5,6,7,8-tetrahydropyrido[4',3':4,5]thieno[2,3-d]pyrimidin-4(3H)-one

Guidance literature:: With sodium amide; In toluene; at 20 ℃; for 24h;
DOI:10.1007/s11172-012-0052-3

Reference yield:

: 1415734-55-2
ethyl 2-anilinomethylideneamino-6-isopropyl-4,5,6,7-tetrahydrothieno[2,3-c]pyridine-3-carboxylate

: 1415734-77-8
dimethyl 1-isopropyl-6'-methylidene-4'-oxo-3'-phenyl-3',4',5,6-tetrahydro-1H-spiro[pyridine-4,5'-thieno[2,3-d]pyrimidine]-2,3-dicarboxylate

: 1415735-07-7
dimethyl 7-isopropyl-4-oxo-3-phenyl-3,4,5,6,7,10-hexahydropyrimido[5',4':4,5]thieno[3,2-d]azocine-8,9-dicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium amide / toluene / 24 h / 20 °C

2: acetonitrile / 288 h / 20 °C

With sodium amide; In toluene; acetonitrile; 2: |Stevens Rearrangement;
DOI:10.1007/s11172-012-0052-3