bis-(3,5-di-tert-butyl-2-oxo-phenyl)-oxamido-bis-(diphenylgermane)

Base Information

Chemical Name:bis-(3,5-di-tert-butyl-2-oxo-phenyl)-oxamido-bis-(diphenylgermane)
CAS No.:1001428-16-5
Molecular Formula:C₅₄H₆₀Ge₂N₂O₄
Molecular Weight:946.261
Hs Code.:

Synonyms:bis-(3,5-di-tert-butyl-2-oxo-phenyl)-oxamido-bis-(diphenylgermane)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis-(3,5-di-tert-butyl-2-oxo-phenyl)-oxamido-bis-(diphenylgermane)

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Technology Process of bis-(3,5-di-tert-butyl-2-oxo-phenyl)-oxamido-bis-(diphenylgermane)

There total 1 articles about bis-(3,5-di-tert-butyl-2-oxo-phenyl)-oxamido-bis-(diphenylgermane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.5%

: 36931-29-0
1,2-bis(3,5-di-tert-butyl-2-hydroxyphenyl)oxamide

: 1613-66-7
dichlorodiphenylgermane

: 1001428-16-5
bis-(3,5-di-tert-butyl-2-oxo-phenyl)-oxamido-bis-(diphenylgermane)

Guidance literature:: With triethylamine; In tetrahydrofuran; byproducts: (CH3)3N*HCl; addn. dropwise via syringe NEt3 to soln. of (HOC6H2(C(CH3)3)2NHCO)2 in THF at 0°C for 1 h; addn. dropwise of GePh2Cl2 at -78°C; warming to room temp. and stirring for 18 h; evapn. of solvent in vac., washing of residue twice with cold THF; crystn.; elem. anal.;
DOI:10.1016/j.jorganchem.2007.08.042