N~1~,N~2~-Bis(3,5-di-tert-butyl-2-hydroxyphenyl)ethanediamide

Base Information

Chemical Name:N~1~,N~2~-Bis(3,5-di-tert-butyl-2-hydroxyphenyl)ethanediamide
CAS No.:36931-29-0
Molecular Formula:C30H44N2O4
Molecular Weight:496.69
Hs Code.:
DSSTox Substance ID:DTXSID50574004
Nikkaji Number:J1.349.452E
Wikidata:Q82462869
Mol file:36931-29-0.mol

Synonyms:DTXSID50574004;N~1~,N~2~-Bis(3,5-di-tert-butyl-2-hydroxyphenyl)ethanediamide

Suppliers and Price of N~1~,N~2~-Bis(3,5-di-tert-butyl-2-hydroxyphenyl)ethanediamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of N~1~,N~2~-Bis(3,5-di-tert-butyl-2-hydroxyphenyl)ethanediamide

Chemical Property:

XLogP3:8.3
Hydrogen Bond Donor Count:4
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:496.33010789
Heavy Atom Count:36
Complexity:715

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)(C)C1=CC(=C(C(=C1)NC(=O)C(=O)NC2=CC(=CC(=C2O)C(C)(C)C)C(C)(C)C)O)C(C)(C)C

Technology Process of N~1~,N~2~-Bis(3,5-di-tert-butyl-2-hydroxyphenyl)ethanediamide

There total 4 articles about N~1~,N~2~-Bis(3,5-di-tert-butyl-2-hydroxyphenyl)ethanediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1643-39-6
2-amino-4,6-di-tertbutylphenol

: 95-92-1
oxalic acid diethyl ester

: 36931-29-0
1,2-bis(3,5-di-tert-butyl-2-hydroxyphenyl)oxamide

Guidance literature:: at 80 ℃; for 1.5h;
DOI:10.1016/S0022-328X(00)00689-6

Reference yield: 61.0%

: 79-37-8
oxalyl dichloride

: 1643-39-6
2-amino-4,6-di-tertbutylphenol

: 36931-29-0
1,2-bis(3,5-di-tert-butyl-2-hydroxyphenyl)oxamide

Guidance literature:: With triethylamine; In diethyl ether; at 0 - 20 ℃;
DOI:10.1002/ejic.200200516

Reference yield:

: 3383-21-9
3,5-di-tert-butyl-o-benzoquinone

: 36931-29-0
1,2-bis(3,5-di-tert-butyl-2-hydroxyphenyl)oxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 75 percent / 1,2-ethylenediamine / H₂O; propan-2-ol / 2 h / Heating

2: 80 percent / 1.5 h / 80 °C

With ethylenediamine; In water; isopropyl alcohol;
DOI:10.1016/S0022-328X(00)00689-6