C₂₉H₃₅NO₈

Base Information

Chemical Name:C₂₉H₃₅NO₈
CAS No.:931581-24-7
Molecular Formula:C₂₉H₃₅NO₈
Molecular Weight:525.599
Hs Code.:

C<sub>29</sub>H<sub>35</sub>NO<sub>8</sub>

Synonyms:C₂₉H₃₅NO₈

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Chemical Property of C₂₉H₃₅NO₈

Chemical Property:

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Technology Process of C₂₉H₃₅NO₈

There total 13 articles about C₂₉H₃₅NO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 103-82-2
phenylacetic acid

: 620970-65-2
((3S,4R,7R,8R,9S)-7-Butyl-8-hydroxy-4,9-dimethyl-2,6-dioxo-[1,5]dioxonan-3-yl)-carbamic acid benzyl ester

: 931581-24-7
C₂₉H₃₅NO₈

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;
DOI:10.1002/ejoc.201100034

Reference yield:

: 931581-19-0
C₂₀H₃₀O₅

: 931581-24-7
C₂₉H₃₅NO₈

Guidance literature:: Multi-step reaction with 9 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h / 0 - 20 °C

2: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.5 h / 20 °C

3: dmap; triethylamine / toluene / 16 h / 0 - 20 °C

4: hydrogenchloride; water / ethanol / 24 h / 20 °C

5: pyrrolidine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triphenylphosphine / acetonitrile / 7 h / 0 - 20 °C

6: triphenylphosphine / toluene / 3 h / 20 °C

7: copper(I) trifluoromethanesulfonate benzene / benzene / 3 h / 80 °C

8: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C

9: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

With pyrrolidine; hydrogenchloride; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) trifluoromethanesulfonate benzene; water; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; ethanol; dichloromethane; toluene; acetonitrile; benzene;
DOI:10.1002/ejoc.201100034

Reference yield:

: 931581-20-3
C₂₉H₅₀O₅Si

: 931581-24-7
C₂₉H₃₅NO₈

Guidance literature:: Multi-step reaction with 8 steps

1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.5 h / 20 °C

2: dmap; triethylamine / toluene / 16 h / 0 - 20 °C

3: hydrogenchloride; water / ethanol / 24 h / 20 °C

4: pyrrolidine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; triphenylphosphine / acetonitrile / 7 h / 0 - 20 °C

5: triphenylphosphine / toluene / 3 h / 20 °C

6: copper(I) trifluoromethanesulfonate benzene / benzene / 3 h / 80 °C

7: pyridine hydrogenfluoride / tetrahydrofuran / 3 h / 20 °C

8: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

With pyrrolidine; hydrogenchloride; dmap; tetrakis(triphenylphosphine) palladium⁽⁰⁾; copper(I) trifluoromethanesulfonate benzene; water; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; ethanol; dichloromethane; toluene; acetonitrile; benzene;
DOI:10.1002/ejoc.201100034