Technology Process of C23H18N6O2
There total 8 articles about C23H18N6O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C24H20N6O2;
With
boron fluoride-dimethyl sulfide complex;
In
dichloromethane;
at 20 ℃;
for 16h;
With
sodium hydrogencarbonate;
In
dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: selenium(IV) oxide / 1,4-dioxane / 60 °C
2: ethanol / 2 h / Reflux
3: [bis(acetoxy)iodo]benzene / 1 h / 20 °C
4: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate / water; 1,2-dimethoxyethane / 0.75 h / 140 °C / Microwave irradiation
5: boron fluoride-dimethyl sulfide complex / dichloromethane / 16 h / 20 °C
With
selenium(IV) oxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; [bis(acetoxy)iodo]benzene; boron fluoride-dimethyl sulfide complex; potassium carbonate;
In
1,4-dioxane; 1,2-dimethoxyethane; ethanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: [bis(acetoxy)iodo]benzene / 1 h / 20 °C
2: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate / water; 1,2-dimethoxyethane / 0.75 h / 140 °C / Microwave irradiation
3: boron fluoride-dimethyl sulfide complex / dichloromethane / 16 h / 20 °C
With
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; [bis(acetoxy)iodo]benzene; boron fluoride-dimethyl sulfide complex; potassium carbonate;
In
1,2-dimethoxyethane; dichloromethane; water;
