Technology Process of C25H17ClO
There total 4 articles about C25H17ClO which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
(methoxymethyl)triphenylphosphonium chloride;
With
potassium tert-butylate;
In
tetrahydrofuran; diethyl ether;
at 20 ℃;
for 1h;
C23H13ClO;
In
tetrahydrofuran; diethyl ether;
at 20 ℃;
for 5h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sulfuric acid / ethanol / 0.5 h / 0 °C
1.2: 1 h / 0 °C
1.3: 5 h / Reflux
2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 4 h / 90 °C
3.1: potassium tert-butylate / diethyl ether; tetrahydrofuran / 1 h / 20 °C
3.2: 5 h / 20 °C
With
sulfuric acid; potassium tert-butylate; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; diethyl ether; ethanol; water; toluene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 4 h / 20 °C
2.1: sulfuric acid / ethanol / 0.5 h / 0 °C
2.2: 1 h / 0 °C
2.3: 5 h / Reflux
3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; ethanol; water / 4 h / 90 °C
4.1: potassium tert-butylate / diethyl ether; tetrahydrofuran / 1 h / 20 °C
4.2: 5 h / 20 °C
With
N-Bromosuccinimide; sulfuric acid; potassium tert-butylate; sodium carbonate;
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; diethyl ether; ethanol; water; N,N-dimethyl-formamide; toluene;