benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-methylidene-2-N-(trans-2-pentenoyl)-β-D-allopyranoside

Base Information

Chemical Name:benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-methylidene-2-N-(trans-2-pentenoyl)-β-D-allopyranoside
CAS No.:434949-25-4
Molecular Formula:C₂₆H₂₉NO₆
Molecular Weight:451.519
Hs Code.:

Synonyms:benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-methylidene-2-N-(trans-2-pentenoyl)-β-D-allopyranoside

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Chemical Property of benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-methylidene-2-N-(trans-2-pentenoyl)-β-D-allopyranoside

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Technology Process of benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-methylidene-2-N-(trans-2-pentenoyl)-β-D-allopyranoside

There total 6 articles about benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-methylidene-2-N-(trans-2-pentenoyl)-β-D-allopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 434948-89-7
benzyl (R)-4,6-O-benzylidene-2-deoxy-2-(trans-2-pentenamido)-β-D-allopyranoside

: 74-95-3
1,1-dibromomethane

: 434949-25-4
benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-methylidene-2-N-(trans-2-pentenoyl)-β-D-allopyranoside

Guidance literature:: With sodium hydroxide; tetrabutylammomium bromide; In dichloromethane; water; for 48h; Heating;
DOI:10.1016/S0957-4166(01)00562-6

Reference yield:

: 13991-37-2
trans-2-pentenoic acid

: 434949-25-4
benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-methylidene-2-N-(trans-2-pentenoyl)-β-D-allopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / triethylamine; pentachlorophenol trichloroacetate / tetrahydrofuran / 8 h / 20 °C

2: 90 percent / NaOH; tetrabutylammonium bromide / CH₂Cl₂; H₂O / 48 h / Heating

With sodium hydroxide; trichloroacetic acid pentachlorophenyl ester; tetrabutylammomium bromide; triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/S0957-4166(01)00562-6

Reference yield:

: 195006-98-5
benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-β-D-allopyranoside

: 434949-25-4
benzyl 2-amino-(R)-4,6-O-benzylidene-2-deoxy-2-N-3-O-methylidene-2-N-(trans-2-pentenoyl)-β-D-allopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / triethylamine; pentachlorophenol trichloroacetate / tetrahydrofuran / 8 h / 20 °C

2: 90 percent / NaOH; tetrabutylammonium bromide / CH₂Cl₂; H₂O / 48 h / Heating

With sodium hydroxide; trichloroacetic acid pentachlorophenyl ester; tetrabutylammomium bromide; triethylamine; In tetrahydrofuran; dichloromethane; water;
DOI:10.1016/S0957-4166(01)00562-6