methyl (2S)-4-({[(1Z)-amino(phenyl)methylene]amino}oxy)2-[(tert-butoxycarbonyl)amino]-4-oxobutanoate

Base Information

Chemical Name:methyl (2S)-4-({[(1Z)-amino(phenyl)methylene]amino}oxy)2-[(tert-butoxycarbonyl)amino]-4-oxobutanoate
CAS No.:220050-46-4
Molecular Formula:C₂₃H₂₇N₃O₆
Molecular Weight:441.484
Hs Code.:

Synonyms:methyl (2S)-4-({[(1Z)-amino(phenyl)methylene]amino}oxy)2-[(tert-butoxycarbonyl)amino]-4-oxobutanoate

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Chemical Property of methyl (2S)-4-({[(1Z)-amino(phenyl)methylene]amino}oxy)2-[(tert-butoxycarbonyl)amino]-4-oxobutanoate

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Technology Process of methyl (2S)-4-({[(1Z)-amino(phenyl)methylene]amino}oxy)2-[(tert-butoxycarbonyl)amino]-4-oxobutanoate

There total 1 articles about methyl (2S)-4-({[(1Z)-amino(phenyl)methylene]amino}oxy)2-[(tert-butoxycarbonyl)amino]-4-oxobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13512-57-7
N-[(1,1-dimethylethoxycarbonyl)amino]-L-asparagine benzyl ester

: 613-92-3
N-hydroxybenzamidine

: 220050-46-4
methyl (2S)-4-({[(1Z)-amino(phenyl)methylene]amino}oxy)2-[(tert-butoxycarbonyl)amino]-4-oxobutanoate

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 18h;

Reference yield: 88.0%

: 220050-46-4
C₂₃H₂₇N₃O₆

: 220050-67-9
(2S)-2-tert-butoxycarbonylamino-3-(3-phenyl-[1,2,4]oxadiazol-5-yl)-propionic acid benzyl ester

Guidance literature:: at 114 ℃; Neat (no solvent);
DOI:10.1016/j.bmcl.2011.03.109

Reference yield:

: 220050-46-4
C₂₃H₂₇N₃O₆

: 719308-40-4
(2S)-2-amino-3-(3-phenyl-[1,2,4]oxadiazol-5-yl)-propionic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 114 °C / Neat (no solvent)

2: trifluoroacetic acid / dichloromethane

With trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmcl.2011.03.109