(η3-allyl)chloro(3-methyl-1,4-bis(2,4,6-trimethylphenyl)-1,2,3-triazol-5-ylidene)palladium(II)

Base Information

Chemical Name:(η3-allyl)chloro(3-methyl-1,4-bis(2,4,6-trimethylphenyl)-1,2,3-triazol-5-ylidene)palladium(II)
CAS No.:1370328-77-0
Molecular Formula:C₂₄H₃₀ClN₃Pd
Molecular Weight:502.395
Hs Code.:

Synonyms:(η3-allyl)chloro(3-methyl-1,4-bis(2,4,6-trimethylphenyl)-1,2,3-triazol-5-ylidene)palladium(II)

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Chemical Property of (η3-allyl)chloro(3-methyl-1,4-bis(2,4,6-trimethylphenyl)-1,2,3-triazol-5-ylidene)palladium(II)

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Technology Process of (η3-allyl)chloro(3-methyl-1,4-bis(2,4,6-trimethylphenyl)-1,2,3-triazol-5-ylidene)palladium(II)

There total 1 articles about (η3-allyl)chloro(3-methyl-1,4-bis(2,4,6-trimethylphenyl)-1,2,3-triazol-5-ylidene)palladium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: bis(η3-allyl-μ-chloropalladium(II))

: 1263862-40-3
3-methyl-1,4-bis(2,4,6-trimethylphenyl)-1H-1,2,3-triazolium tetrafluoroborate

: 20667-12-3
silver(l) oxide

: 1370328-77-0
(η3-allyl)chloro(3-methyl-1,4-bis(2,4,6-trimethylphenyl)-1,2,3-triazol-5-ylidene)palladium(II)

Guidance literature:: With (CH₃)4NCl; In dichloromethane; acetonitrile; under N2, Schlenk tube; Ag2O (0.12 mmol) and Me4NCl (0.22 mmol) added tosoln. of C2HN3(Me)(Mes)2BF4 (0.22 mmol) in MeCN/CH2Cl2 (1/1), mixt. sti rred at room temp. for 5 h, (PdCl(allyl))2 (0.11 mmol) added, mixt. stirred overnight; evapn. under vac., residue extd. with CH2Cl2, extract filtered, filtrateconcd., chromy. (SiO2, 20% EtOAc/hexanes), recrystn. from CH2Cl2/hexane ; elem. anal.;
DOI:10.1002/ejic.201101383